In case it is desired to weigh the extract it may be done directly by
weighing it in the test-tube T after drying in the usual way at the
end of the extraction; or a glass flask H, made to fit freely into the
test-tube, may be used, in which case a little mercury is poured into
the bottom of the tube to seal the space between H and T. To prevent
spirting of the substance in H, or projecting any of the extracted
material without or against the bottom of the crucible G, the funnel
represented by the dotted lines in the right hand section may be used.
Heat may be applied to the test-tube either by hot water, or steam, or
by a bunsen, which permits of the flame being turned down to minimum
proportions without danger of burning back. When the test-tube alone
is used it is advisable to first put into it some fragments of pumice
stone, particles of platinum foil, or a spoonful of shot, to prevent
bumping of the liquid when the lamp is used as the source of heat.
Any air which the apparatus contains is pushed out through F when the
boiling begins, the tube F not being closed until the vapor of the
liquid has reached its maximum height. With cold water in the condenser
the vapor of ether very rarely reaches above the lower compartment and
the vapor of alcohol rarely above the second.
When the plate P is accurately turned so as to fit the ground surface
of the mouth of T, it is found that ten cubic centimeters of anhydrous
ether or alcohol are sufficient to make a complete extraction, and
there is not much loss of solvent in six hours. The thickness of the
asbestos film in G, or its fineness, is so adjusted as to prevent too
rapid filtration so that the solvent may just cover the material to
be extracted, or, after the material is placed in a crucible, a plug
of extracted glass wool may be placed above it for the purpose of
distributing the solvent evenly over the surface of the material to be
extracted and of preventing the escape of fine particles.
[Illustration: FIGURE 24. IMPROVED COMPACT EXTRACTION APPARATUS.]
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