Scientific American Supplement, No. 299, September 24, 1881Various
Science
Scientific American Supplement, No. 299, September 24, 1881
Various
Science -- Periodicals
For a same range of temperature between the boiler and the refrigerator,
the weight of alcohol which distills in an hour is constant. By the
operation of the valve, D, it becomes easy to allow all the liquid
condensed in the first refrigerator to pass into the second boiler;
and thus the second rectification, which is effected in a more perfect
vacuum, is supplied with exactness. The object of this valve, then, is
to allow the liquid to pass, and yet to cut off the pressure in such
a way as to have a double fall of temperature throughout the whole
apparatus; from 60° to 20° in the first operation, and from 0° to -40°
in the second. We may add that the regulation of the valve is extremely
easy, because of the screw which actuates it.
To sum up the commercial advantages that our process procures, we may
say that it realizes the following _desiderata_: 1. With the cost of a
single distillation we have, at once, distillation and rectification,
or a single expense for two results. 2. With one operation at a low
temperature we obtain products which are almost impossible to get even
by an indefinite number of rectifications at a high temperature, the
temperature having an intrinsic value in the operation. 3. The alcohols
obtained are wholesome, and can be put on the market without danger. 4.
Their superior quality gives these alcohols an extra value difficult
to calculate, but which is very notable. 5. The whole operation being
performed in closed vessels, there is absolutely no waste. 6. For the
same reason there is scarcely any danger of fire. 7. The management of
the works and the service are performed by the pressure of the gases
entirely; there are only a few cocks to be turned to perform all the
interior maneuvers, empty and fill the vessels, etc. Hence economy in
_personnel_.
* * * * *
ELECTROLYTIC DETERMINATIONS AND SEPARATIONS.
[Footnote: NOTE.--Each of these determinations was accompanied by a
series of results in which the practical determinations obtained from
the method described were compared with the theoretical contents of the
solutions of the various elements. These, however, would take up too
much room for insertion in these columns.]
By ALEX. CLASSEN and M.A. VON REIS; translated by M. BENJAMIN, Ph.B.,
F.C.S.
Public-domain text, read in full here on John Shaqi.
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