Scientific American Supplement, No. 303, October 22, 1881 — John Shaqi
Scientific American Supplement, No. 303, October 22, 1881Various
Science
Scientific American Supplement, No. 303, October 22, 1881
Various
Science -- Periodicals
All the tubing of the pump is supported at a distance of about 55 mm.
from the wood-work; this is effected by the use of simple adjustable
supports and adjustable clamps; the latter have proved a great
convenience. The object is to gain the ability to heat with a Bunsen
burner all parts of the pump without burning the wood-work. Where glass
and wood necessarily come in contact the wood is protected by metal or
simply painted with a saturated solution of alum. The glass portions
of the pump I have contrived to anneal completely by the simple means
mentioned below. If the glass is not annealed it is certain to crack
when subjected to heat, thus causing vexation and loss of time. The
mercury was purified by the same method that was used by W. Siemens
(Pogg. Annalen, vol. ex., p. 20), that is, by a little strong sulphuric
acid to which a few drops of nitric acid had been added; it was dried by
pouring it repeatedly from one hot dry vessel to another, by filtering
it while quite warm, the drying being completed finally by the action of
the pump itself. All the measurements were made by a fine cathetometer
which was constructed for me by William Grunow; see this Journal, Jan.,
1874, p. 23. It was provided with a well-corrected object-glass having a
focal length of 200 mm. and as used by me gave a magnifying power of 16
diameters.
_Manipulation_.--The necessary connections are effected with a cement
made by melting Burgundy pitch with three or four per cent of gutta
percha. It is indispensable that the cement when cold should be so hard
as completely to resist taking any impression from the finger nail,
otherwise it is certain to yield gradually and finally to give rise to
leaks. The connecting tubes are selected so as to fit as closely as
possible, and after being put into position are heated to the proper
amount, when the edges are touched with a fragment of cold cement which
enters by capillary attraction and forms a transparent joint that can
from time to time be examined with a lens for the colors of thin plates,
which always precede a leak. Joints of this kind have been in use by me
for two months at a time without showing a trace of leakage, and the
evidence gathered in another series of unfinished experiments goes to
show that no appreciable amount of vapor is furnished by the resinous
compound, which, I may add, is never used until it has been repeatedly
melted. As drying material I prefer caustic potash that has been in
fusion just before its introduction into the drying tube; during the
process of exhaustion it can from time to time be heated nearly to the
melting point: if actually fused in the drying tube the latter almost
invariably cracks. The pump in the first instance is to be inclined at
an angle of about 10 degrees, the tube of the gauge being supported by
a semicircular piece of thick pasteboard fitted with two corks into the
top of the cylinder. This seemingly awkward proceeding has in no case
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