The Manufacture of Paper: With Illustrations, and a Bibliography of Works Relating to Cellulose and Paper-MakingSindall, R. W. (Robert Walter)
History
The Manufacture of Paper: With Illustrations, and a Bibliography of Works Relating to Cellulose and Paper-Making
Sindall, R. W. (Robert Walter)
Papermaking
Cellulose 48·25
Water 9·38
Aqueous extract 10·19
Pectous matter 26·39
Fatty matter 2·07
Ash 3·72
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100·0
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Yield of dry cellulose obtained in actual practice
from good raw material 45 to 48%
By boiling the esparto with caustic soda under pressure for a stated
time, the non-fibrous constituents are removed, leaving the cellulose
in a more or less pure form according to the severity of the chemical
treatment.
[Illustration: FIG. 20.--An Esparto Duster.]
In practice the grass is packed tightly into upright stationary
digesters and a definite quantity of caustic soda solution added,
the amount of chemical used being equal to 15-18 per cent. of the
weight of grass packed into the digester. The form of digester almost
universally employed is that known as the Sinclair's "vomiting" boiler,
which is constructed so that a continuous circulation of the liquid
is maintained by means of what are called "vomit" pipes. These are
fitted to the sides of the digester in such a manner that the caustic
soda solution circulates from the bottom of the digester, up through
the "vomit" pipes, and is discharged downwards upon the contents of
the boiler through a perforated plate fixed in the upper part of the
digester. The requisite quantity of caustic soda solution is placed in
the digester, and steam admitted into the bottom of the vessel while
the grass is being thrown in. In this way a much larger weight of grass
can be boiled at one operation, since the bulk is greatly reduced when
the grass has become thoroughly soft and wet.
[Illustration: FIG. 21.--Sinclair's "Vomiting" Esparto Boiler.]
When the boiler is loaded the inlet is closed up and steam turned on
to the full pressure of about 40 or 50 lbs., this being maintained
for a period of about four hours. The non-fibrous constituents of the
esparto are gradually dissolved out by the caustic soda, and when the
operation is completed the black liquor is run off from the digester
into large store tanks, and the esparto grass which remains in the
digester is then completely washed until the soda is almost entirely
washed out.
[Illustration: FIG. 22.--A Porion Evaporator.]
Public-domain text, read in full here on John Shaqi.
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