A Journey Through France in War TimeButler, Joseph G. (Joseph Green)
History
A Journey Through France in War Time
Butler, Joseph G. (Joseph Green)
France -- Description and travel; World War, 1914-1918
Chloride of Lime (bleaching powder) 25% CI act....200 gr.
Sodium Carbonate, dry (Soda of Solway) 100 gr.
Sodium Bi-carbonate....80 gr.
Pour into 12 litre flask the two hundred grammes of chloride of
lime and five litres of ordinary water, shake vigorously for a few
minutes and leave in contact for six to twelve hours, one night for
example. (Shake until dissolved) at least the big pieces are
dissolved, large pieces float--notice only floating pieces. At the
same time, dissolve in five litres of cold ordinary water the
carbonate and bi-carbonate of soda.
After leaving from six to twelve hours, pour the salt solution in
the flask containing the macerated chloride of lime, shake
vigorously for a few minutes and leave to allow the calcium
carbonate to be precipitated. In about half an hour, siphon the
liquid and filter with a double paper to obtain a good, clear
liquid, which should always be kept in a dark place.
Tritration of Chloride of Lime (Bleaching Powder).
Because of the variation of the products now obtained in the
market, it is necessary to determine the quantity of active
chlorine contained in the chloride of lime which is to be used.
This, in order to employ an exact calculated quantity according to
its concentration. The test is made in the following manner:--
Take from different parts of the bar a small quantity of beaching
powder to have a medium sample, weigh 20 grammes of it, mix as well
as possible in a litre of tap water and leave in contact for a few
hours. Measure 10 c.c. of the clear liquid and add 20 c.c. of a 10%
solution of potassium iodide, 2 c.c. of acetic acid or hydrochloric
acid, then put drop by drop into the mixture a decinormal solution
of sodium hyposulfite (2.48%) until decoloration. The number "N"
of cubic centimeters of hyposulfite employed multiplied by 1,775
will give the weight "N" of active chloride contained in 100
grammes of chloride of lime.
The test must be made every time a new product is received. When
the result obtained will differ more or less than 25%, it will be
necessary to reduce or enlarge the proportion of the three products
contained in the preparation. This can be easily obtained by
multiplying each of the three numbers--200, 100, 60 by the factor
N/25 in which N represents the weight of the active chlorine per
cent of chloride of lime.
Measure 10 c.c. of the solution, add 20 c.c. of potassium iodide
1/10, 2 c.c. of acetic acid and drop by drop a decinormal solution
of sodium hyposulfite until decoloration. The number of cubic
centimeters used multiplied by 0.03725 will give the weight of the
hypochlorite of soda contained in 100 c.c. of the solution.
Never heat the solution and if in case of urgency one is obliged to
resort to trituration of chloride of lime in a mortar, only employ
water, never salt solution.
Test of Thetalkalinity of Dakin Solution:--
Public-domain text, read in full here on John Shaqi.
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