A Practical Handbook on the Distillation of Alcohol from Farm ProductsWright, F. B. (Frederic B.)
Science
A Practical Handbook on the Distillation of Alcohol from Farm Products
Wright, F. B. (Frederic B.)
Alcohol; Alcohol, Denatured
In Germany, the de-naturing law passed in 1887 was so framed as to
maintain the high revenue tax on alcohol intended for drinking, but to
exempt from taxation such as should be de-naturized and used for
industrial purposes. De-naturing is accomplished by mixing with the
spirit a small proportion of some foreign substance, which, while not
injuring its efficiency for technical uses, renders it unfit for
consumption as a beverage. The de-naturing substances employed depend
upon the use to which the alcohol is to be subsequently applied. They
include pyridin, picolin, benzol, toluol, and xylol, wood vinegar, and
several other similar products. As a result of this system Germany
produced and used last year 100,000,000 gallons of de-natured spirits, as
compared with 10,302,630 gallons used in 1886, the last year before the
enactment of the present law.
The following are some of the other de-naturants used in Germany:
Camphor, oil of turpentine, sulphuric ether, animal oil, chloroform,
iodoform, ethyl bromide, benzine, castor oil, lye.
* * * * *
In France the standard mixture consists of:
150 liters of Ethyl alcohol,
15 liters of wood alcohol,
1/2 liter of heavy benzine,
1 gram. Malachite green.
An illustration of de-naturing on a large scale is given by the methods
and operations of a large London establishment. On the ground floor are
four large iron tanks holding about 2500 gallons each. On the next floor
are casks of spirit brought under seal from the bonded warehouse. On the
third floor are the wood alcohol tanks, and on the fourth floor cans of
methylating materials. On the fourth floor the covers to the wood alcohol
tanks were removed (these tank covers were flush with that floor) and the
contents gauged and tested. The quantity to be put into the tanks on the
first floor was run off through pipes connecting with the first-floor
tanks and the upper tanks relocked. Then going to the second floor, each
cask of the grain spirit was gauged and tested and the tank covers, which
were flush with the floor, were removed and the casks of the grain spirit
were run into the tanks below. The mixture was then stirred with
long-handled wooden paddles and the tank covers replaced, and the
material was ready for sale free of tax. The mixture was 10 per cent.
wood alcohol and 90 per cent. ethyl alcohol made from molasses, and was
what is known as the ordinary methylating spirit used for manufacturing
purposes only and used under bond. The completely de-natured spirit is
made by adding to the foregoing three-eighths of one per cent. of
benzine.
This benzine prevents re-distillation.
In the United States there are at present two general formulas for
de-natured alcohol in use, either one of which may be used by any
manufacturer, who can use de-natured alcohol.
Public-domain text, read in full here on John Shaqi.
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