A Practical Handbook on the Distillation of Alcohol from Farm ProductsWright, F. B. (Frederic B.)
Science
A Practical Handbook on the Distillation of Alcohol from Farm Products
Wright, F. B. (Frederic B.)
Alcohol; Alcohol, Denatured
The grain to be mashed, which has been ground and steeped as before
described, is mixed with malt in the proportion of four to one, or even
eight to one. In addition, three or four pounds of chaff to every hundred
or so pounds of steeped grain should be used.
=Mash.= Water is then run into the mash tub in the proportion of about
600 gallons to each 60 bushels of grain. Its temperature should be
between 120∞ and 150∞ F. During the entrance of water, the mass is well
stirred so as to cause the whole of the grain to be thoroughly soaked and
to prevent the formation of lumps. It is best to add the grain to the
water gradually and to stir thoroughly.
To this mass about 400 gallons of boiling water is gradually added to
keep the temperature at about 145∞ F. During the addition of the boiling
water the mash should be continually stirred so that the action of the
water shall be uniform. This operation should last about two and one half
hours. The vat should be then covered and left to stand from
three-quarters to one hour for saccharification.
Another method of saccharifying is to turn boiling water gradually into
the mash tank until the mixture has acquired a temperature of from 140∞
to 180∞ F. The mass is thoroughly stirred and the tub is covered and left
to subside for from two to four hours, during which time the temperature
should not be allowed to fall below 120∞ F. A small tub needs more heat
than a larger tub, and more heat is required in winter than in summer.
A convenient method of regulating the temperature of the mash tank, would
be by a coil of pipes on the bottom. This would be connected by a two-way
cock to a steam boiler and to a source of cold water. Heat should never
be carried over 180∞ F., and the best temperature is from 145∞ to 165∞ F.
The greatest effect of the diastase of the malt upon the gelatinized
starch is at 131∞ F. For ungelatinized starch this is not great enough,
hence the greater part of the mashing is carried on at the lower
temperature and only towards the end should the temperature be raised to
the maximum 150∞ F.
Every distiller uses his own judgment as to the amount of the mashing
water used, its temperature, the length of time during which the mash
rests, and the length of time for saccharification.
Saccharification may be recognized by the following signs: The mash loses
its first white mealy look, and changes to dark brown. It also becomes
thin and easily stirred. The taste is sweet and its odor is like that of
fresh bread.
Corn and other grain may be mashed conveniently in such an apparatus as
that described on page 10, as used for potatoes the steam being
introduced under pressure.
The water is first placed in the steamer. Steam is introduced into the
water and it is brought to a boil. The corn is then introduced gradually,
the steam pressure increased to its maximum, and the mass blown out as
described in Chapter VII. Hellefreund's apparatus (see page 118) may also
be used with ground corn.
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