A practical treatise on the manufacture of perfumery : $b comprising directions for making all kinds of perfumes, sachet powders, fumigating materials, dentrifices, cosmetics, etc., etc., with a full account of the volatile oils, balsams, resins, and other natural and artificial perfume-substances, including the manufacture of fruit ethers, and tests of their purityDeite, C. (Carl)
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A practical treatise on the manufacture of perfumery : $b comprising directions for making all kinds of perfumes, sachet powders, fumigating materials, dentrifices, cosmetics, etc., etc., with a full account of the volatile oils, balsams, resins, and other natural and artificial perfume-substances, including the manufacture of fruit ethers, and tests of their purity
Deite, C. (Carl)
Cosmetics; Perfumes; Perfumes industry
Alcohol is added either by itself or in the form of saturated
solution of storax, benzoin, or Canada balsam, by which means the
specific gravity of the balsam is but slightly changed. Bring the
above-mentioned common salt solution, together with 20 grammes of the
Peru balsam to be examined, into a small flask, and distil off about 5
grammes; gradually mix the distillate with 5 drops of caustic potash
lye and potassium iodide solution saturated with iodine, shaking gently
until the mixture acquires a slightly yellow-brownish coloration. If
this coloration does not disappear in one minute, add drop by drop
more of the potash lye until discoloration appears. In the presence
of alcohol, yellow crystals of iodoform, which are readily recognized
under the microscope by their form, collect on the bottom of the fluid.
Adulteration with a volatile oil is recognized in the distillate by
odor and taste.
Fat oil, Canada balsam, copaiba balsam, gurjun balsam, and volatile
oil may be recognized by the following tests: If pure Peru balsam in
a porcelain saucer is thoroughly mixed with an equal volume of pure
concentrated sulphuric acid, the mixture thereby becomes heated, vapors
of a pungent odor being emitted, and if then set aside to cool, it
congeals. In the presence of fat or volatile oils, copaiba balsam,
gurjun balsam, or Canada balsam, it remains, however, more or less
thickly fluid or more or less soft-smeary. If the balsam be pure, the
cold mixture, after washing with water, should yield a hardish or
soft-friable mass, which, when kneaded with the fingers, should not
prove smeary or sticky.
Fat oils are also very readily recognized by the use of warm
petroleum-ether. The extract is evaporated, saponified with potash lye,
extracted with alcohol, evaporated and decomposed with hydrochloric
acid. A mixture of cinnamic acid and any of the fatty acids present in
the Peru balsam is thereby obtained, which, after treatment with water,
remains in the residue.
Public-domain text, read in full here on John Shaqi.
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