A System of Instruction in the Practical Use of the Blowpipe: Being A Graduated Course Of Analysis For The Use Of Students And All Those Engaged In The Examination Of Metallic CombinationsAnonymous
Science
A System of Instruction in the Practical Use of the Blowpipe: Being A Graduated Course Of Analysis For The Use Of Students And All Those Engaged In The Examination Of Metallic Combinations
Anonymous
Blowpipe
(7) with carb. soda. The alkali is absorbed into the charcoal,
leaving an infusable mass which gives the sulfur
reaction on silver.
(8) Special reactions. If not containing too much iron or manganese
gives an alumina reaction with nitrate of of
cobalt. In other respects as the preceding.
* * * * *
Mineral. Turquoise
Formula. [...Al=]^{2}[.....P] + 5[.H].
Behavior
(1) in glass-bulb. Evolves water, occasionally decrepitates and
turns black.
(2) in open tube. --
(3) on charcoal. Turns brown, but remains infusible.
(4) in forceps. V. As on charcoal. Colors the outer flame green.
(5) in borax. In the oxidizing flame, gives a green bead, due
to copper and iron. In reducing flame, opaque red.
(6) in mic. salt. As in borax.
(7) with carb. soda. Intumesces, then fuses to a semi-clear glass
colored by iron. With more alkali yields an
infusible mass.
(8) Special reactions. Gives the phosphoric-acid reaction.
* * * * *
Mineral. Wavellite
Formula. [Al=]F^{3} + 3([...Al=]^{4}[.....P]^{3} + 18[.H].)
Behavior
(1) in glass-bulb. Evolves water and some fluorine, which attacks
the glass.
(2) in open tube. --
(3) on charcoal. Exfoliates and turns white.
(4) in forceps. V. As on charcoal. Colors the outer flame green,
especially if moistened with SO^{3}.
(5) in borax. As alumina. Generally gives also a slight iron
reaction.
(6) in mic. salt. As in borax.
(7) with carb. soda. Forms an infusible white mass.
(8) Special reactions. With cobalt-solution on charcoal gives the
alumina reaction.
* * * * *
Mineral. Spinel
Formula. [.R][...Al=].
Behavior
(1) in glass-bulb. --
(2) in open tube. --
(3) on charcoal. --
(4) in forceps. V.
(5) in borax. Gives a slight iron reaction.
(6) in mic. salt. As in borax.
(7) with carb. soda. Fuses partially and forms a porous mass.
(8) Special reactions. With nitrate of cobalt gives the alumina
reaction. With nitre and carbonate of soda a
slight manganese reaction.
* * * * *
SILICATES.
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