A System of Instruction in the Practical Use of the Blowpipe: Being A Graduated Course Of Analysis For The Use Of Students And All Those Engaged In The Examination Of Metallic CombinationsAnonymous
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A System of Instruction in the Practical Use of the Blowpipe: Being A Graduated Course Of Analysis For The Use Of Students And All Those Engaged In The Examination Of Metallic Combinations
Anonymous
Blowpipe
(8) Special reactions. Generally gives the manganese reaction with
nitre and carbonate of soda.
* * * * *
Mineral. Chloropal
Formula. [...Fe=][...Si]^{2} + 3[.H].
Behavior
(1) in glass-bulb. Decrepitates more or less, gives off much water
and turns black.
(2) in open tube. --
(3) on charcoal. --
(4) in forceps. V. Loses color and turns black.
(5) in borax. Gives the iron reaction.
(6) in mic. salt. Gives the iron and silica reaction.
(7) with carb. soda. Fuses to a transparent green glass.
(8) Special reactions. --
* * * * *
Mineral. Green earth
Formula. [...Si],[.Fe],[...Al=],[.Na],[.K],[.H], etc.
Behavior
(1) in glass-bulb. Gives off water and becomes darker in color.
(2) in open tube. --
(3) on charcoal. --
(4) in forceps. V. In reducing flame fuses on edges and colors
the outer flame yellow ([.Na]) or violet ([.K]).
(5) in borax. As the preceding.
(6) in mic. salt. As the preceding.
(7) with carb. soda. Forms a slaggy mass.
(8) Special reactions. --
* * * * *
Mineral. Siderite
Formula. [.Fe][..C].
Behavior
(1) in glass-bulb. Occasionally decrepitates. Gives off CO^{2} and
turns black and magnetic.
(2) in open tube. --
(3) on charcoal. As in glass bulb.
(4) in forceps. Behaves similarly to the magnetic oxide.
(5) in borax. Gives the iron and manganese reaction.
(6) in mic. salt. As in borax.
(7) with carb. soda. Behaves as an oxide. With nitre and carbonate of
soda on platinum generally gives the manganese
reaction.
(8) Special reactions. In acid dissolves with effervescense.
* * * * *
Mineral. Copperas
Formula. [.Fe][...S] + 7[.H].
Behavior
(1) in glass-bulb. Gives off water, and, when strongly heated,
SO^{2} and SO^{3}, which reddens litmus paper.
(2) in open tube. Evolves water and SO^{2}, which may be
recognized by its odor.
(3) on charcoal. Loses water and SO^{2}, and is converted into
[...Fe=].
(4) in forceps. Gives off H and SO^{2}, and then behaves as the
magnetic oxide.
(5) in borax. The roasted mineral affords an iron reaction.
(6) in mic. salt. As in borax.
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