A system of pyrotechny : $b Comprehending the theory and practice, with the application of chemistry; designed for exhibition and for war.Cutbush, James
History
A system of pyrotechny : $b Comprehending the theory and practice, with the application of chemistry; designed for exhibition and for war.
Cutbush, James
Fireworks; Military fireworks
The sulphur of commerce is commonly of three different colours, viz:
citron-yellow, deep yellow, and brownish-yellow. These colours depend
on the different degrees of heat to which the sulphur was exposed,
in its extraction. The operation of refining consists in conducting
the fire in such a manner, as that the colour of the sulphur will
assume a brilliant yellow, bordering on a green. We must, therefore,
to produce this effect, operate on the sulphur according to its
colour. For the green sulphur, as little heat has been used for its
extraction, the fire may be left under the boiler until there is no
more left to melt than the top. The sulphur of the yellow colour may
be kept longer on the fire, which may be removed when the mass is
melted three-fourths. The sulphur of a brown colour, being already
much burnt, may be removed when the mass is melted one-half. If it
is required to operate on all the varieties at the same time, in
order to produce sulphur of a uniform colour, in that case we must
fill the boiler one-half with the green sulphur, one-fourth with the
yellow, and the remainder with the brown, and removing the fire when
the yellow is almost wholly melted. The boiler is then covered with
a lid. The fusion is completed by the heat of the mass. The light
bodies then raise themselves to the surface, forming a black scum,
which is removed, and the heavy bodies fall to the bottom. The boiler
remains for four or five hours, uncovering it from time to time to
take off the scum. The fluid part is removed, and is suffered to
congeal, taking care not to disturb the deposite.
The second process of refining is by sublimation. This operation
consists in subliming it in a close apparatus, which in sulphur
refineries are boilers placed in brick work, and furnished with
heads. These heads communicate by a pipe with a vaulted chamber,
placed at some distance from the furnace. The chamber serves to
collect the sulphur. There is usually a stone slab fixed between
the chamber and the head. The chamber is furnished with one or two
iron-plate valves. There is an opening in the head of each boiler,
in order to renew the sulphur: it is closed very tight by a plate of
iron. There is an opening also in the chamber, to admit a person,
which is closed likewise by an iron plate. The heads are luted before
the process is commenced.
By this process the sulphur is refined; for the pure part is
sublimed, and the foreign substances remain in the pots. The product
thus obtained is the ordinary flowers of sulphur. If the heat be
moderate, the sublimation is more perfect. It is necessary at
the same time that the temperature of the chamber should be low,
otherwise the sulphur will melt, which frequently takes place. Coarse
particles are separated from the flour, should they occur, by a sieve.
Public-domain text, read in full here on John Shaqi.
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