A text-book of assaying : $b for the use of those connected with mines.Beringer, C. (Cornelius)
Science
A text-book of assaying : $b for the use of those connected with mines.
Beringer, C. (Cornelius)
Assaying
In some cases the fusion of the ore may be replaced by a treatment with
solution of cyanide of potassium and the gold recovered from the
solution in the way just described. For this purpose the ore should be
in not too fine powder, otherwise there will be great difficulty in
filtering; a sand which will pass a 30 sieve and having no large
proportion of very fine stuff will do. Not less than 200 grams should be
taken; and as an extraction apparatus a bell jar capable of holding half
as much again may be used. Such a jar may be extemporised by cutting off
the bottom of a bottle by leading a crack around it with a red hot
poker; or a lamp chimney will serve the purpose. The smaller mouth of
the jar is closed by a perforated cork provided with a clipped tube
after the manner of a burette (see fig. 44c). In the jar, just over
the cork, put a plug of loose asbestos or glass wool, or a piece of
sponge to act as a filter; a layer of broken glass, coarse at the bottom
and fine at the top, will serve the same purpose. On this, place the
charge of ore to be extracted. Prepare a solution of cyanide of
potassium in water, with 5 or 10 grams of the salt to the litre. It may
be that the whole point of the assay depends on the solution being of a
definite strength; as, for example, where the relative efficiency of
solutions of different strengths is being determined, when it will be
best to estimate the quantity of cyanide of potassium in the dilute
solution by the method given at the end of this article (page 160). Pour
the cyanide solution on to the ore, letting the first portions to come
through run into the beaker, but as soon as the ore is thoroughly wetted
close the clip and allow to stand for several hours. Then, opening the
clip, run through more cyanide solution and then water, so as to wash
the gold-carrying liquor thoroughly into the beaker. It is no matter if
the liquor is a little bit turbid; transfer it to a lead dish,
evaporate, scorify, and cupel in the usual fashion.
The assay of gold-zinc slimes, which is the precipitate formed by zinc
acting on cyanide solutions of gold, may be made by wrapping 2 or 3
grams in 40 grams of sheet lead and scorifying, cupelling, &c. The
amount of impurity in the stuff varies greatly; it is usually calcined
and mixed thoroughly with soda 40 per cent., borax 30 per cent., and
sand 10 per cent., and melted in graphite pots. The buttons of bullion
obtained are afterwards remelted with borax and run into bars, the
fineness of which varies from 600 to 830 thousandths. The bars are
sampled by chipping off diagonally opposite corners: or better, by
drilling, the drillings being freed from pieces of steel with the help
of a magnet.
Public-domain text, read in full here on John Shaqi.
Reviews
Reviews
No reviews yet
Be the first to share your thoughts on this work.
Elsewhere in the archive
Join the Discussion
Join the discussion
Sign in to leave a comment or review.
Sign InorCreate an account