A text-book of assaying : $b for the use of those connected with mines.Beringer, C. (Cornelius)
Science
A text-book of assaying : $b for the use of those connected with mines.
Beringer, C. (Cornelius)
Assaying
~Parting in special apparatus.~--One plan for obtaining greater
uniformity is to stamp each cornet with a number for purposes of
identification, and to treat several, including one or more check assays
in the same acid contained in a beaker; all the assays under these
conditions evidently receive precisely the same acid treatment. Such a
plan can of course only be adopted where there is no risk of the gold
breaking up during the parting. An improvement on this is to have a
porcelain basin[29] about 8-1/2 inches in diameter and with a capacity
of about 1-1/2 litres. It is provided with a porcelain cover with 30
numbered holes through which tubes dip into the acid. The cover is
removable. The tubes are like test-tubes and are supported by the cover;
their bottoms are perforated with holes or slits. The acid is placed in
the basin and boiled over a flat burner; it enters the tubes through the
slits. The cornets are placed each in its proper tube. When the boiling
is finished, the cover with the tubes is lifted and at the same time the
acid drains back into the basin. A dip into a basin of distilled water
washes at one operation all 30 assays. The cover is then put on a basin
containing the stronger parting acid which is already boiling. This
boiling is continued for half an hour. The cover with the 30 cornets is
then lifted out from the acid and dipped two or three times in distilled
water to wash off the last traces of acid. To transfer the cornets from
the tubes to the porous cups the whole of the tube must be dipped under
the water; otherwise the operation is exactly as when working with
test-tubes.
A still simpler method of working is to use small platinum cups[30]
provided with fine slits which admit the acid but retain the gold. A
number of these, say 60, are supported on a platinum tray. The parting
acids are boiled in platinum dishes under a hood; and the 60 cornets
(each in its proper cup) are placed in the acid all at once: the tray
carrying the cups is provided with a handle suitable for this purpose.
After a proper boiling the tray is lifted out of the weaker acid into
the stronger one, where it undergoes the second boiling. It is next
dipped several times in distilled water and lastly, after a gentle
drying, it is raised to an annealing temperature which must not be too
high for fear of the gold sticking to the platinum. After cooling, the
cornets are transferred from the platinum cups directly to the pan of
the balance. Here all 60 cornets have exactly the same treatment and the
"checks" may be compared with great exactness with the other assays
accompanying them. There is, too, a great saving of labour.[31]
Public-domain text, read in full here on John Shaqi.
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