A text-book of assaying : $b for the use of those connected with mines.Beringer, C. (Cornelius)
Science
A text-book of assaying : $b for the use of those connected with mines.
Beringer, C. (Cornelius)
Assaying
~The electrodes~ consist of a platinum spiral and cylinder. The spiral
should have the shape shown in A, fig. 54. When in work it is passed
through one of the holes fitted with glass tubes and connected with the
copper end of the battery. The thickness of the wire of which it is made
is unimportant, provided it is stout enough to keep its form and does
not easily bend. The spiral will weigh about 8 grams. The cylinder (C,
fig. 54) will weigh about 12 grams. It should have the shape shown in
the figure. In working it is clamped to one of the terminals, and on it
the copper is deposited. A cylinder will serve for the deposition of
from 1 to 1.5 gram of copper. It is made by rivetting a square piece of
foil on to a stiff piece of wire, and then bending into shape over a
glass tube or piece of rounded wood. Each cylinder carries a distinctive
number, and is marked by impressing Roman numerals on the foil with the
blade of a knife. The weight of each is carefully taken and recorded.
They lose slightly in weight when in use, but the loss is uniform, and
averages half a milligram per month when in daily use. The cylinders are
cleaned from deposited copper by dissolving off with nitric acid and
washing with water; and from grease by igniting.
The ~beakers~, to contain the solution of copper to be electrolysed, are
ordinary tall beakers of about 200 c.c. capacity, and are marked off at
100 c.c. and 150 c.c. They are supported on movable stands, consisting
of wooden blocks about six inches high and three inches across. The bar
of wood which carries the connecting wires and electrodes is permanently
fixed over the working bench, at such a height that, with the beakers
resting on these blocks, the electrodes shall be in position for
working.
To fix the electrodes to the rod, remove the stand and beaker and pass
the long limb of the spiral up through one of the glass tubes. Connect
it with the free end of the copper spiral by means of a connecting screw
(fig. 52), and then draw out and bend the copper spiral so that the
platinum one may hang freely. Screw the wire of the cylinder to the
terminal, and, if necessary, bend it so that the cylinder itself may be
brought to encircle the rod of the spiral in the manner shown in fig.
53.
The ~general method of working~ is as follows:--The quantity of ore to
be taken for an assay varies with the richness of the ore, as is shown
in the following table:--
Percentage of Copper Quantity of Ore
in the Ore. to be taken.
1 to 5 5 grams
5 to 10 3 "
10 to 30 2 "
30 to 50 1.5 "
50 to 100 1 "
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