A text-book of assaying : $b for the use of those connected with mines.Beringer, C. (Cornelius)
Science
A text-book of assaying : $b for the use of those connected with mines.
Beringer, C. (Cornelius)
Assaying
When a clay crucible is used, the method of working is as
follows:--Weigh up 25 grams of the dry and powdered ore, mix with an
equal weight of "soda" and 2 grams of tartar; place in a crucible (E.
Battersea round), and then insert a piece of iron rod about half an inch
in diameter, and of such a length that it will just allow the crucible
to be covered. The rod should be pushed down so as to touch the bottom
of the crucible, and the mixture should be covered with a sprinkling of
borax. Place in a furnace heated to, but not above, redness, and cover
the crucible. In about twenty minutes the charge will be fused: the
fusion is complete when bubbles of gas are no longer being evolved; and
then, but not till then, the iron is withdrawn, any adhering buttons of
lead being washed off by dipping the rod a few times in the slag. Cover
the crucible, leave it for a minute or two, and then pour. Detach the
slag, when cold, by hammering. The weight of the button multiplied by 4
gives the percentage. The commoner errors of students in working the
process are too high a temperature and too quick a withdrawal.
A sample of ore treated in this manner gave on duplicate assay 17.5 and
17.6 grams of lead, equalling 70.0 and 70.4 per cent. respectively. By
wet assay the sample gave 73.3 per cent. Using an iron crucible, the
results will be 1 per cent. or so higher. The crucible must be made of
wrought iron; and, if it has been previously used, should be cleaned by
heating to dull redness and scraping the scale off with a stirrer. Take
30 grams of the ore, mix with 30 grams of "soda" and 3 grams of tartar;
put the mixture in the crucible, and cover with a sprinkling of borax;
heat for about twenty minutes at not too high a temperature, and then
scrape down the slag adhering to the side with a stirrer. Leave in the
furnace till action has ceased. Before pouring, tap the pot gently, and
then tilt it so as to make the slag wash over the part of the crucible
along which the charge is to be poured. Pour; and, when cold, clean and
weigh the button of metal. A crucible may be used from ten to twenty
times.
These assays are for ores containing the lead chiefly as sulphide. For
oxidised ores, charcoal or tartar is employed as the reducing agent. The
student may practise on red lead as follows:--Take 30 grams of red lead;
mix with 10 grams each of borax and "soda" and about 1.5 gram of
powdered charcoal; place in a small clay crucible with a cover (C.
Battersea round), fuse at a gentle heat, and pour when action ceases.
This assay will only take a few minutes.
Public-domain text, read in full here on John Shaqi.
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