A text-book of assaying : $b for the use of those connected with mines.Beringer, C. (Cornelius)
Science
A text-book of assaying : $b for the use of those connected with mines.
Beringer, C. (Cornelius)
Assaying
~Cornish Method.~--_Tin Ore Assay._--The ore to be smelted or assayed
should be concentrated to say not less than 50 per cent. of metallic
tin; though to obtain satisfactory results it should be brought nearer
70 per cent., as with ore containing less than 40 to 50 per cent. of
metal there will be a considerable loss both in the assaying and in the
smelting. If the ore to be operated on does not contain this quantity of
metal, then the sample (if coarse) must be reduced to a fine state, the
gangue being removed by vanning, and the ore saved for the fire assay.
The method adopted for the determination of tin in the ore is as
follows:--About 2-1/2 ounces troy (1200 grains, or about 80 grams) of
the ore to be assayed is weighed out and mixed on a flat copper pan
(shaped with a long lip) with one-fifth of its weight (240 grains, or
15.5 grams) of powdered culm (anthracite). The mixture of ore and culm
is either transferred to a black-lead crucible before the latter is put
into the furnace, or, as some prefer, it is carefully swept into a
crucible which has been imbedded in the fire. Some assayers cover their
pots with a flat cover placed loosely on, while others leave the mixture
in the open pot. The furnace, which has been previously fired to a
strong heat, is then covered, and the sample is subjected to a sharp
fire for a period of from twelve to twenty minutes. No definite time can
be stated, as, besides the strength of the fire, the quality and
condition of the ore, and the impurities associated with it, greatly
affects the time required for the complete reduction of the ore. As soon
as the mixture in the crucible has settled down to a uniform white heat,
and any very slight ebullition which may have taken place has subsided,
the crucible is gently shaken, removed from the fire (the culm-ash or
slag which covers the metal being carefully drawn aside with an iron
scraper), and the metal is poured quickly into an iron ingot-mould,
which is usually placed on a copper pan to save the culm-slag and the
adherent metal which comes out with it. The crucible is then carefully
scraped, and the scrapings, together with the contents of the mould and
pan, are transferred to a mortar. There the ingot of tin is freed from
slag and then taken to the scales. The rest, after being finely
powdered, is passed through a sieve. The flattened particles of tin
which remain on the sieve are weighed with the ingot (the _lump_, as it
is called); whilst the siftings are vanned on a shovel, and (the slag
being washed off) the fine tin is collected, dried, and weighed with the
rest: the whole gives the produce or percentage of metal in the ore.
The results of the assays are expressed in cwts. of metal in the ton of
ore. The percentage is rarely given and never used in Cornwall.
Thus--"13-1/2 Produce" would mean that the assay yielded results at the
rate of 13-1/2 cwts. of metal for one ton of the ore. Some assayers use
Public-domain text, read in full here on John Shaqi.
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