Cooley's Cyclopædia of Practical Receipts and Collateral Information in the Arts, Manufactures, Professions, and Trades..., Sixth Edition, Volume ICooley, Arnold James
Science
Cooley's Cyclopædia of Practical Receipts and Collateral Information in the Arts, Manufactures, Professions, and Trades..., Sixth Edition, Volume I
Cooley, Arnold James
Formulas, recipes, etc.; Industrial arts -- Dictionaries; Technology -- Dictionaries
_Gen. commentary._ The selection of any one of the processes given above
for the preparation of alcohol must greatly depend on the convenience or
position of the operator. Chloride of calcium, and quick-lime, from their
powerful affinity for water, and easy application, are the hygrometric
substances most generally employed; but the processes involving the use of
the other substances and methods already noticed, have all of them
advantages under particular circumstances. Gay-Lussac has recommended the
use of caustic baryta instead of lime; and others have employed dry
alumina, as an absorbent of the water prior to distillation. Common proof
spirit may be concentrated until its sp. gr. falls to about 0·825, by
simple distillation in a water bath; at which sp. gr. it contains only
about 11% of water, by weight, and is then nearly as volatile as pure
alcohol.
A convenient apparatus for the preparation of alcohol, on the small
scale, is that figured in the _engr._, and which will be self-explanatory
to every one competent to use it. The tank (_i_) should be supplied with
ice-cold water; and the receiver (_g_) should be covered with cloths kept
continually wet with water of the same temperature. The capsule or basin
(_c_) is a water bath heated by the little gas furnace (_d_). On the large
scale, for commercial alcohol, a copper still, fitted with a glass
refrigeratory and receiver, is commonly employed.
By surrounding the capital of a still, or other like apparatus, by a water
bath kept at the proper temperature, the alcoholic richness or content of
the product may be regulated to the greatest nicety, for any desired
strength.
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