Elements of the Theory and Practice of Chymistry, 5th ed.Macquer, Pierre Joseph
History
Elements of the Theory and Practice of Chymistry, 5th ed.
Macquer, Pierre Joseph
Chemistry -- Early works to 1800
The ash-hole is terminated at its upper end, like that of the
reverberating furnace, by a grate, which serves for the bottom of
the fire-place, and ought to be very substantial, that it may resist
the violence of the fire. The inside of this furnace is commonly an
elliptic curve; because it is demonstrated by mathematicians that
surfaces having that curvature reflect the rays of the sun, or of fire,
in such a manner, that meeting in a point, or a line, they produce
there a violent heat. But, to answer this purpose, those surfaces must
be finely polished; an advantage hardly procurable to the internal
surface of this furnace, which can be made of nothing but earth:
besides, if it were possible to give it a polish, the violent action of
the fire that must be employed in this furnace would presently destroy
it. Yet the elliptical figure must not be entirely disregarded: for,
if care be taken to keep the internal surface of the furnace as smooth
as possible, it will certainly reflect the heat pretty strongly, and
collect it about the center.
The fire-place of this furnace ought to have but four apertures.
First, that of the lower grate, which communicates with the ash-hole.
Secondly, a door in its fore-side, through which may be introduced
coals, crucibles, and tongs for managing them: this aperture should be
made to shut exactly with a plate of iron, having its inside coated
with earth, and turning on two hinges fixed to the furnace.
Thirdly, over this door a hole slanting downwards, towards the place
where the crucible is to stand. The use of this hole is to give the
operator an opportunity of examining the condition of the matters
contained in his crucible without opening the door of the fire-place:
this hole should be made to open and shut easily, by means of a stopple
of earth.
Fourthly, a circular aperture of about three inches wide in the upper
part or vault of the furnace, which should gradually lessen and
terminate, like that of the dome of the reverberating furnace, in a
short conical funnel of about three inches long, and fitted to enter
the conical pipe before described, which is applied when the activity
of the fire is to be increased.
When this furnace is to be used, and a crucible to be placed in it,
care must be taken to set on the grate a cake of baked earth, somewhat
broader than the foot of the crucible. The use of this stand is to
support the crucible, and raise it above the grate, for which purpose
it should be two inches thick. Were it not for this precaution the
bottom of the crucible, which would stand immediately on the grate,
could never be thoroughly heated, because it would be always exposed to
the stream of cold air which enters by the ash-hole. Care should also
be taken to heat this earthen bottom red-hot before it be placed in the
furnace, in order to free it from any humidity, which might otherwise
happen to be driven against the crucible during the operation, and
occasion its breaking.
Public-domain text, read in full here on John Shaqi.
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