Elements of the Theory and Practice of Chymistry, 5th ed.Macquer, Pierre Joseph
History
Elements of the Theory and Practice of Chymistry, 5th ed.
Macquer, Pierre Joseph
Chemistry -- Early works to 1800
"M. Geoffroy, having put his Sedative Salt made by crystallization to
all the same trials with that made by sublimation, satisfied himself
that there is no other difference between the two. If the Sedative Salt
made by crystallizations happens to calcine in the sun; that is, if its
lustre tarnishes, and its surface grows mealy, it is a sign that it
still contains either a little Borax or some Glauber's Salt: for these
two Salts are apt to calcine in this manner, and pure Sedative Salt
should not be subject to this inconvenience. In order to purify it, and
free it entirely from those Salts, it must be dissolved once more in
boiling water. As soon as the water cools, the Sedative Salt reappears
in light, shining, crystalline plates, swimming in the liquor. After
standing four and twenty hours, the liquor must be decanted, and the
salt washed with fresh water; by which means it will be very pure and
beautiful."
Glauber's Salt and Borax dissolve in water with vastly more ease than
the Sedative Salt, and consequently do not crystallize so readily by
much: so that the small portion of those salts which may have been left
on the surface of the Sedative Salt, being diffused through a large
quantity of water, continues in a state of solution, while the Sedative
Salt crystallizes; which being also washed afterwards with fair water,
it is impossible that the smallest particle of those other Salts
should remain adhering to it; and consequently this must be deemed an
excellent way of purifying it.
SECTION II.
_Of Operations on_ METALS.
CHAP. I.
_Of_ GOLD.
PROCESS I.
_To separate Gold, by Amalgamation with Mercury, from the Earth and
Stones with which it is found mixed._
Pulverize the earths and stones containing Gold. Put the powder into a
little wooden tray; dip this tray in water, gently shaking it and its
contents. The water will grow muddy, by taking up the earthy parts of
the ore. Continue washing it in this manner till the water cease to
appear turbid. Upon the ore thus washed pour strong vinegar, having
first dissolved therein, by the help of heat, about a tenth part of its
weight of alum. The powder must be quite drenched and covered with this
liquor, and so left to stand for twice twenty-four hours.
Decant the vinegar, and wash your powder with warm water, till the
last that comes off hath no taste: then dry it, and put it into an
iron mortar, with four times its weight of Quick-silver: triturate the
whole with a heavy wooden pestle, till all the powder be of a blackish
colour: then pour in a little water, and continue rubbing for some time
longer. More earthy and heterogeneous particles will be separated from
the metalline parts by means of this water, which will look dirty: it
must then be decanted, and more fair water added. Repeat this several
times; then dry what remains in the mortar with a sponge, and by the
help of a gentle heat: you will find it an Amalgam of the Mercury with
the Gold.
Public-domain text, read in full here on John Shaqi.
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