Food Adulteration and Its Detection: With photomicrographic plates and a bibliographical appendixBattershall, Jesse P. (Jesse Park)
Science
Food Adulteration and Its Detection: With photomicrographic plates and a bibliographical appendix
Battershall, Jesse P. (Jesse Park)
Food adulteration and inspection; Food adulteration and inspection -- United States
The estimation of the ash is made by evaporating 100 c.c. of the sample
in a weighed platinum dish to dryness, and incinerating the residue at
a rather moderate heat, so as to avoid volatilisation of the chlorides.
The amount of ash in normal beer should never exceed 0·5 per cent.,
the usual proportion being about 0·3 per cent.; this would naturally
be increased by the addition of sodium bicarbonate or sodium chloride
to the beer. The complete analysis of the ash is seldom necessary, but
it is often of importance to estimate the amount of sodium chloride
contained. This is effected by dissolving the ash-residue in distilled
water and precipitating the chlorine from an aliquot portion of the
solution by silver nitrate; one part of the precipitate obtained
represents 0·409 part of common salt. The proportion of sodium
chloride in pure beer is very inconsiderable, but it may be added to
the beverage either to improve the flavour or to create thirst. For
the determination of phosphoric acid, a weighed portion of the ash
is dissolved in nitric acid, the solution evaporated to dryness, and
the residue boiled with water containing a little nitric acid. It is
then filtered, concentrated by evaporation, an excess of ammonium
molybdate solution added, and the mixture set aside for about ten
hours, after which the precipitate formed is separated by filtration
and dissolved in ammonium hydroxide. A solution of magnesium sulphate
(mixed with a considerable quantity of ammonium chloride) is now added,
and the precipitated ammonio-magnesium phosphate collected, washed,
ignited, and weighed, 100 parts of this precipitate contain 64 parts of
phosphoric anhydride (P_{2}O_{5}).
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