Food Adulteration and Its Detection: With photomicrographic plates and a bibliographical appendixBattershall, Jesse P. (Jesse Park)
Science
Food Adulteration and Its Detection: With photomicrographic plates and a bibliographical appendix
Battershall, Jesse P. (Jesse Park)
Food adulteration and inspection; Food adulteration and inspection -- United States
2. _Total solid residue and loss on ignition._--500 c.c. of the water
under examination are introduced, in small portions at a time, into a
tared platinum dish, and evaporated to dryness over the water-bath, the
residue being subsequently dried for three or four hours in an air-bath
at 100°. The solid residue obtained, multiplied by 200, represents
parts in 100,000: or, by 140, grains per imperial gallon. It is usually
considered that, unless the proportion of total solids exceeds 40
grains per Imperial gallon (32 grains per U.S. gallon, or about 56·5
parts per 100,000), the water need not be objected to for drinking
purposes on this ground alone. The volatile and organic matters are
determined by igniting the solid residue, which is afterwards allowed
to cool. It is then moistened with a little carbonic acid water or
solution of ammonium carbonate, dried to constancy at 130°, and the
organic matter estimated by the decrease in weight. Formerly, this
process was chiefly depended upon for determining the proportion of
organic substances contained in water. It is open to numerous serious
objections, among which are, that it may afford a result either
below or above that correctly representing the quantity of organic
ingredients present in the sample. The first case takes place when
a portion of the organic matter is decomposed during the process of
evaporation, and is quite liable to occur; the second case takes place
when the water contains nitrates, which would be decomposed upon
ignition. The method, however, possesses some value, and is still often
resorted to as affording a general idea of the proportion of organic
contamination present, the degree of blackening of the solid residue
during the process of ignition being, at least, a useful qualitative
indication.
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