Food Adulteration and Its Detection: With photomicrographic plates and a bibliographical appendixBattershall, Jesse P. (Jesse Park)
Science
Food Adulteration and Its Detection: With photomicrographic plates and a bibliographical appendix
Battershall, Jesse P. (Jesse Park)
Food adulteration and inspection; Food adulteration and inspection -- United States
Regarding the addition of mineral acids to vinegar in the United
States, it is satisfactory to note that, of a large number of samples
tested by the New York City Vinegar Inspector during the past year, not
a single sample was found to contain these adulterants.
Fermented infusions of molasses, “black strap,” etc., are occasionally
employed in the manufacture of vinegar. The product obtained from these
sources has been found in some instances to contain acrid and probably
noxious ingredients.
FOOTNOTES:
[133] Archiv. der Pharm., 1876, p. 193.
[134] Pharm. Centralb., N.F. 7, p. 292.
[135] Dingl. Poly. Journ., 256, p. 129.
PICKLES.
The examination of pickles naturally includes a determination of the
character of the vinegar used in their preparation. This is made by
the methods just described. The practice of imparting a bright green
colour to pickles which have become bleached by long preservation in
brine or by other means, is doubtless still prevalent, and calls for
a brief notice. The greening of pickles is effected either by the
direct addition of cupric sulphate to the water in which they are
heated, or by introducing some form of metallic copper into the bath.
Alum is stated to be also occasionally employed for the same purpose.
The presence of copper is readily detected by incinerating a rather
considerable quantity of the pickles, treating the ash with a little
nitric acid and adding an excess of ammonium hydroxide to the solution,
when, in presence of the metal, a blue coloration will be produced.
The quantitative estimation of copper is made by boiling the residue,
obtained by the evaporation of the vinegar or the incineration of the
pickles, with dilute nitric acid, adding a small quantity of sulphuric
acid and expelling the excess of nitric acid by evaporating nearly to
dryness. The solution is next diluted with water, filtered, and the
filtrate placed in a platinum capsule. The copper is then deposited by
electrolysis. In the Report of the Brooklyn Board of Health for the
year 1885, a case is recorded where a child ate a portion of a pickle
coloured with cupric sulphate (containing an estimated quantity of 2½
grains of the salt), with fatal results.
OLIVE OIL.
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