Food Adulteration and Its Detection: With photomicrographic plates and a bibliographical appendixBattershall, Jesse P. (Jesse Park)
Science
Food Adulteration and Its Detection: With photomicrographic plates and a bibliographical appendix
Battershall, Jesse P. (Jesse Park)
Food adulteration and inspection; Food adulteration and inspection -- United States
“In the ground spices it will be found more difficult to recognise
the anatomy of the parts than in a carefully prepared section. The
hardest parts are often the largest particles, and scarcely at all
transparent. The mounting of the material in water or glycerine will
render them more so, but it is necessary to employ some other means of
which two are available. A solution of chloral hydrate in water, 8 to
5, serves after 24 hours to make the particles less obscure. In many
instances also, it has been found advisable to bleach the deep colour
by Schulze’s method, using nitric acid of 1·1 sp. gr. and chlorate of
potash. When this is done, hard tissue is broken down and rendered
transparent where otherwise nothing could be seen. As examples, olive
stones and cocoa-nut shells will serve. Without treatment little can be
made out of their structure.
“Of course, it is plain that the detection of starch must be in a
portion of the material which has received no treatment, and that
progress must be made from the least to the most violent reagents.
“For this work an elaborate microscope is unnecessary. It should, for
work with starches, have objectives of ½ and 1/5 inch equivalent focus,
arrangements for polarising light, and if possible, a condenser system.
Many good stands are to-day made at reasonable prices which will serve
the purpose.”
The microscopical appearance of various starches in polarised light is
shown in Plate IX. Plate XII. exhibits several spices, under polarised
light, in a pure and adulterated state. Those represented are:--
Ginger, pure, and adulterated with foreign starch.
Cinnamon and Cassia; the pure barks, ground, showing the relative
greater frequency of fibro-vascular bundles in the former.
Cayenne, pure, and adulterated with rice starch.
The chemical analysis of spices, although usually of minor importance,
often serves to confirm the results secured by aid of the microscope.
The principal determinations required are the ash, oil, starch, and
sugar. The more common forms of spice adulteration are the following:--
_Cloves._--This spice is said to be sometimes deprived of its volatile
oil before being put on the market. In the genuine article the
proportion of oil seldom falls below 17 per cent. The oil is readily
estimated by distilling the suspected sample with water. The usual
adulterants of ground cloves consist of clove-stems, allspice, flour
and burnt shells.
PLATE XII.
[Illustration: Ginger Starch.]
[Illustration: Ginger Adulterated.]
[Illustration: Cinnamon.]
[Illustration: Cassia.]
[Illustration: Cayenne.]
[Illustration: Cayenne Adulterated.]
SPICES.
_Mace._--True mace is frequently mixed with the false spice, the
presence of which is indicated by its dark-red colour. The other
foreign substances most commonly used are turmeric, wheaten flour,
rice, corn meal, and roasted beans.
_Cinnamon._--The chief admixtures to be sought for are cassia, ground
shells, crackers, etc.
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