Food Adulteration and Its Detection: With photomicrographic plates and a bibliographical appendixBattershall, Jesse P. (Jesse Park)
Science
Food Adulteration and Its Detection: With photomicrographic plates and a bibliographical appendix
Battershall, Jesse P. (Jesse Park)
Food adulteration and inspection; Food adulteration and inspection -- United States
then evaporated fully to dryness over boiling water, the number of
grammes weight gained by the dish, when multiplied by ten, gives the
percentage of solid residue contained in the vinegar.
There are certain characteristics peculiar to the residue of a pure
cider vinegar, the principal of which are the following:--It will be
about 3 per cent. in weight, and never less than 2 per cent. It is
always soft, viscid, of apple flavour, somewhat acid and astringent in
taste. A drop of it taken up in a clean loop of platinum or of iron
wire, and ignited in a colourless Bunsen gas-lamp flame, imparts to
it the pale lilac colour of a pure potash salt, without any yellow,
due to sodium, being visible. The ignited residue left in the loop of
wire will be a fusible bead of quite a good size, and it will have
a strong alkaline reaction upon moistened test-paper, effervescing
briskly when immersed in an acid. The presence in a vinegar of the
_slightest_ trace of any free mineral acid will prevent the ignited
residue having any alkaline reaction, or effervescing with acids. The
presence of any practical amount of commercial acetic acid added to
“tone up” the strength of the vinegar will cause the igniting residue
to impart another colour to the Bunsen flame, and the residue itself
will have a smoky pyroligneous taste or odour. Any corn glucose
used in the vinegar will cause its residue when ignited to emit the
characteristic odour of burning corn, and, as the last spark glows
through the carbonised mass, to usually emit the familiar garlic
odour of arsenic, for the common oil of vitriol usually used in the
production of glucose is now mostly derived from pyrites, which almost
always contain arsenic. A glucose vinegar which has been made without
vaporising the alcohol after the fermentation of the glucose will
also have a strong reducing action upon a copper salt in an alkaline
solution, and also will give a heavy precipitation of lime with
ammonium oxalate. A true malt vinegar always contains phosphates, and
a wine vinegar cream of tartar. The presence of any acrid vegetable
substance in a vinegar is known by the residue having a pungent taste,
especially if before the evaporation the vinegar has been exactly
neutralised with soda.
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