Food Adulteration and Its Detection: With photomicrographic plates and a bibliographical appendixBattershall, Jesse P. (Jesse Park)
Science
Food Adulteration and Its Detection: With photomicrographic plates and a bibliographical appendix
Battershall, Jesse P. (Jesse Park)
Food adulteration and inspection; Food adulteration and inspection -- United States
But if the tube, filled with a sugar
solution, is placed in the instrument, the right-handed rotary power
of this substance is added to that half of the double quartz plate
which exerts the same rotary effect (the other half being diminished
in a like degree), and the two divisions of the plate will now appear
of different colours. In order to restore an equilibrium of colour
the movable wedge-shaped quartz plate E is slid along its fellow F by
means of the ratchet M, until the right-handed rotary power of the
sugar solution is compensated for by the increased thickness of the
left-handed plate, when the sections of the plate C will again appear
uniform in colour. For the purpose of measuring the extent to which the
unfixed plate has been moved, a small ivory scale is attached to this
plate, and passes along an index scale connected with the fixed plate.
The degrees marked on the scale, which are divided into tenths, are
read by aid of a mirror _s_ attached to a magnifying glass K. When the
polariscope is in what may be termed a state of equilibrium, _i. e._
before the tube containing the sugar solution has been placed in it,
the index of the fixed scale points to the zero of the movable scale.
In the practical use of the Ventzke-Scheibler saccharimeter the
method to be followed is essentially as follows: 26·048 grammes of
the sugar to be tested are carefully weighed out and introduced into
a flask 100 cubic centimetres in capacity; water is added, and the
flask shaken until all crystals are dissolved. The solution is next
decolorised by means of basic plumbic acetate, its volume made up to
100 cubic centimetres, and a little bone-black having been added if
necessary, a glass tube, corresponding to P (Fig. 3) which is exactly
200 millimetres in length, and is provided with suitable caps, is
completely filled with the clear filtered liquid. This is then placed
in the polariscope, and protected from external light by closing the
cover shown at _h´_. On now observing the field of vision by means of
the telescope, it will be seen that the halves into which it is divided
exhibit different colours. The screw M is then turned to the right
until this is no longer the case, and absolute uniformity of colour is
restored to the divisions of the double quartz plate C (Fig. 2). The
extent to which the screw has been turned, which corresponds to the
right-handed rotation caused by the sugar solution, is now ascertained
on reading the scale by the aid of the glass K. The instrument under
consideration is so constructed that, when solutions and tubes of the
concentration and length referred to above are used, the reading on the
scale gives directly the percentage of pure crystallisable cane sugar
contained in the sample examined. For instance, if the zero index of
the fixed scale points to 96°·5 on the movable scale, after uniformity
of colour has been obtained, the sample of sugar taken contains 96·5
per cent. of pure cane sugar.
Public-domain text, read in full here on John Shaqi.
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