Minerals in rock sections : $b The practical methods of identifying minerals in rock sections with the microscope, especially arranged for students in technical and scientific schoolsLuquer, Lea McIlvaine
Science
Minerals in rock sections : $b The practical methods of identifying minerals in rock sections with the microscope, especially arranged for students in technical and scientific schools
Luquer, Lea McIlvaine
Petrology -- Laboratory manuals
Minerals, such as amphibole, pyroxene, epidote, olivine and garnet
(containing iron), may often be separated by an electro-magnet by
regulating its magnetic intensity.[146]
_Separation by Chemical Means._ Very many different methods may be used,
depending on the nature of the work to be accomplished; but they are
generally only reliable in the hands of a good chemist. The material
should be in the state of fine powder.
As an example may be mentioned the treatment with pure concentrated HFl,
by which the minerals of a rock are attacked in a certain sequence, the
feldspars and related minerals first, then the quartz and finally the
ferro-magnesium silicates, such as amphibole, pyroxene, olivine, etc.
MICRO-CHEMICAL REACTIONS.
The first requisite is to bring the substance to be investigated into
solution. This can be done in the case of non-silicates by the ordinary
solvents, while silicates can be decomposed and investigated either by
the methods of Borichy or Behrens. Both methods rest upon the
recognition of the forms, etc., of artificially produced crystals.
The size of a fragment for testing may vary, according to circumstances,
from that of a poppy seed to a pin head. Good results are recorded from
fragments of not more than 0.2–0.7 sq. mm.
The substance to be tested is placed on glass, protected by a film of
balsam, and covered with a spherical drop of the solvent,[147] which
should be allowed to act until all the different elements composing the
sample are in solution (in the case of a very small fragment until it
has all dissolved). Transfer the solution to another protected object
glass, and, after evaporation, the crystallizations characteristic of
the different elements will be seen.
If the evaporation is too rapid and the crystallizations incomplete, the
residue should be redissolved in water, or a very dilute solution of the
solvent employed, transferred to a fresh glass and allowed to
recrystallize.
Borichy’s Method.[148] (Hydrofluosilicic Acid.)
This method has the advantage of simplicity of manipulation and relative
distinctness in results; but on the other hand these results are only
obtained after several hours, and the temperature has an influence on
the crystalline forms obtained. It is well to make the tests in a
temperature of about 15° C.
Put a spherical drop of pure hydrofluosilicic acid[149] on the fragment
and leave it for some hours in damp air until the action has been
sufficient, then transfer it to a dry air bell-glass and allow
evaporation and crystallization to take place.
For the microscopic examination the objective (200–300 diams. best for
these observations) can be protected with glycerine and a mica disc or
thin cover-glass, or the drop can be all evaporated and the crystals
covered with liquid balsam and a cover-glass.
Crystallizations Obtained by Borichy’s Method.
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