Chemical apparatus; Electroplating; Glass blowing and working; Glass coatings; Glass grinding and polishing; Lampwork; Mirrors
This apparatus may appear unnecessarily complex, but it is worth while
to set it up, for it makes the operation of casting a speculum fairly
certain. If the metal is at the right temperature it will form a
uniformly liquid disc inside the ring. The mass sets almost directly,
and as soon as this occurs it is pushed to the edge of the plate and
the metal in the lip broken off by a smart upward tap with a hammer.
The dovetailed bit of iron is knocked downwards and falls off, and the
ring may then be lifted clear of the casting. The object of the
dovetail will now be understood, for without it there is great risk of
breaking into the speculum in knocking the "tail" off.
A box of quite dry sawdust is prepared in readiness for the process of
annealing before the speculum is cast. The box must be a sound wooden
or metal box, and must be approximately air-tight. For a speculum a
foot in diameter the box must measure at least 3 feet both ways in
plan, and be 2 feet 6 inches deep. Half the sawdust is in the box and
is well pressed down so as to half fill it. The other half must be
conveniently ready to hand. As soon as possible after casting, the
speculum is thrown into the box, covered over with the sawdust, and
the lid is put on.
The object in having the box nearly air-tight is to avoid
air-currents, which would increase the rate of cooling. A speculum a
foot in diameter may conveniently take about three days to anneal, and
should be sensibly warm when the box is opened on the fourth day. For
larger sizes longer times will be required. We will say that the
sawdust thickness on each side must be proportional to the dimensions
of the speculum, or may even increase faster with advantage if time is
of no moment.
The process of annealing may be considered successful if the disc does
not fly to pieces in working; it is to be worked on the chilled side.
The object of giving the chill the approximate counterpart form will
now appear; it saves some rough grinding, and causes the finished
surface to be more homogeneous than it would be if the centre were
sunk by grinding through the chilled surface.
In 1889 I learned from Mr. Schneider, Professor Row-land's assistant
at Baltimore, that in casting specula for concave gratings a good deal
of trouble had been saved by carrying out the operation in an
atmosphere consisting mostly of coal gas. It was claimed that in this
way the presence of specks of oxide was avoided. I did not see the
process in operation, but the results attained are known and admired
by all experimenters.
Sec. 71. Grinding and polishing Specula.
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