Chemical apparatus; Electroplating; Glass blowing and working; Glass coatings; Glass grinding and polishing; Lampwork; Mirrors
Sec. 50. As economy of platinum is often of importance, the following
little art will save money and trouble. Platinum is easily caused to
join most firmly to copper--with which, I presume, it alloys--by the
following method. Hold the platinum wire against the copper wire, end
to end, at the tip of the reducing flame of a typical blowpipe--or
anywhere--preferably in the "reducing" part of the oxygas flame; in
a moment the metals will fuse together at the point of contact, when
they may be withdrawn.
Such a joint is very strong and wholly satisfactory, much better than
a soldered joint. If the work is not carried out successfully so that
a considerable drop of copper-platinum alloy accumulates, cut it off
and start again. The essence of success is speed, so that the copper
does not get "burned." If any considerable quantity of alloy is formed
it dissolves the copper, and weakens it, so that we have first the
platinum wire, then a bead of alloy, and then a copper wire fused into
the bead, but so thin just outside the latter that the joint has no
mechanical strength.
Sec. 51. The Art of making Air-light Joints.
Lamp-manufacturers and others have long since learned that when glass
is in question not only are fused joints made as easily as others, but
that they afford the only reliable form of joint. An experimenter who
uses flint glass, has a little experience, an oxygas blow-pipe and a
blowing apparatus, will prefer to make his joints in this way, simply
from the ease with which it may be done. When it comes to making a
tight joint between glass and other substances the problem is by no
means so easy. Thus Mr. Griffiths (Phil. Trans. 1893, p. 380)
failed to make air-tight joints by cementing glass into steel tubes,
using hard shellac, and the tubes fitting closely. These joints were
satisfactory at first, but did not last; the length of the joint is
not stated. The difficulty was finally got over by soldering very
narrow platinum tubes into the steel, and fusing the former into the
glass.
Mr. Griffiths has since used an alloy with success as a cement, but I
cannot discover what it is made from. Many years ago Professor Hittorf
prepared good high vacuum tubes by plugging the ends of glass tubes
with sealing wax merely, though in all cases the spaces to be filled
with wax were long and narrow (Hittorf, Pogg. Ann. 1869, Sec. 5,
English translation, Phys. Soc. p. 113). Again, Regnault
habitually used brass ferules, and cemented glass into them by means
of his mastic, which can still be procured at a low rate from his
instrument-makers (Golan, Paris). Lenard also, in his investigations
on Cathode Rays (Wied. Ann, vol. li. p. 224), made use of sealing
wax covered with marine glue.
Public-domain text, read in full here on John Shaqi.
Reviews
Reviews
No reviews yet
Be the first to share your thoughts on this work.
Join the Discussion
Join the discussion
Sign in to leave a comment or review.
Sign InorCreate an account