Chemical apparatus; Electroplating; Glass blowing and working; Glass coatings; Glass grinding and polishing; Lampwork; Mirrors
In spite of the great improvements made during recent years in the
construction of so-called Geissler vacuum pumps--i.e. pumps in which
a Torricellian vacuum is continually reproduced--I am of opinion that
Sprengel pumps are, on the whole, more convenient for exhausting
Crooke's tubes. A full discussion of the subject of vacuum pumps will
be found in a work by Mr. G. S. Ram (The Incandescent Lamp and its
Manufacture), published by the Electrician Publishing Company, and it
is not my intention to deal with the matter here; the simplest kind of
Sprengel pump will be found quite adequate for our purpose, provided
that it is well made.
Fig. 42 is intended to represent a modification of a pump based on
the model manufactured by Hicks of Hatton Garden, and arranged to suit
the amateur glass-blower. The only point of importance is the
construction of the head of the fall tube, of which a separate and
enlarged diagram is given. The fall tubes may have an internal
diameter up to 2 mm. (two millimetres) and an effective length of 120
cm.
Free use is made of rubber tube connections in the part of the pump
exposed to the passage of mercury. The rubber employed should be
black and of the highest quality, having the walls strengthened by a
layer of canvas. If such tube cannot be easily obtained, a very good
substitute may be made by placing a bit of ordinary black tube inside
another and rather larger bit and binding the outer tube with tape or
ribbon. In any case the tubing which comes in contact with the
mercury should be boiled in strong caustic potash or soda solution for
at least ten minutes to get rid of free sulphur, which fouls the
mercury directly it comes in contact with it. The tubing is well
washed, rinsed with alcohol, and carefully dried.
Fig. 42.
The diagram represents what is practically a system of three Sprengel
pumps, though they are all fed from the same mercury reservoir and run
down into the same mercury receiver. It is much easier to make three
pumps, each with separate pinch cocks to regulate the mercury supply,
than it is to make three jets, each delivering exactly the proper
stream of mercury to three fall tubes.
Sprengel pumps only work at their highest efficiency when the mercury
supply is carefully regulated to suit the peculiarities of each fall
tube, and this is quite easily done in the model figured. Since on
starting the pump the rubber connections have to stand a considerable
pressure, the ends of the tubes must be somewhat corrugated to enable
the rubber to be firmly wired on to them. The best binding wire is the
purest Swedish iron wire, previously annealed in a Bunsen gas flame.
The wire must never be twisted down on the bare rubber, but must
always be separated from it by a tape binding. By taking this
precaution the wire maybe twisted very much more tightly than is
otherwise possible without cutting the rubber.
Public-domain text, read in full here on John Shaqi.
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