Chemical apparatus; Electroplating; Glass blowing and working; Glass coatings; Glass grinding and polishing; Lampwork; Mirrors
The only difficulty in making such a pump as is described lies in the
bending of the heads of the fall tubes. This bending must be done
with perfect regularity and neatness, otherwise the drops of mercury
will not break regularly, or will break just inside the top of the
fall tube, and so obstruct its entrance that at high vacua no air can
get into the tube at all.
The connections at the head of the fall tubes must also be well put on
and the joints blown out so that the mercury in dropping over the head
is not interfered with by the upper surface of the tube. However, a
glance at the enlarged diagram will show what is to be aimed at better
than any amount of description. In preparing the fall tubes it is
generally necessary to join at least two "canes" together. The joint
must be arranged to occur either in the tube leading the mercury to
the head of the fall, or in that part of the fall tube which remains
full of mercury when the highest vacuum is attained. On no account
must the joint be made at the fall itself (at least not by an
amateur), nor in that part of the fall tube where the mercury falls
freely, particularly at its lower end, where the drops fall on the
head of the column of mercury.
When a high vacuum is attained the efficacy of the pump depends
chiefly on the way in which the drops fall on the head of the column.
If the fall is too long the drops are apt to break up and allow the
small bubble of air to escape up the tube, also any irregularity or
dirt in the tube at this point makes it more easy for the bubbles of
air to escape to the surface of the mercury.
Any pump in which the supply of mercury to the fall tube can be
regulated nicely will pump well until the lowest available pressures
are being attained; a good pump will then continue to hold the air
bubbles, while a bad one will allow them to slip back [Footnote: For
special methods of avoiding this difficulty see Mr. Ram's book.] ...
Though three fall tubes are recommended, it must not be supposed that
the pump will produce a Crooke's vacuum three times more rapidly than
one fall tube. Until the mercury commences to hammer in the pump the
three tubes will pump approximately three times faster than one tube,
but as soon as the major portion of the air collected begins to come
from the layer condensed on the glass surface of the tube to be
exhausted and from the electrodes, the rate at which exhaustion will
go on no longer depends entirely on the pump.
Public-domain text, read in full here on John Shaqi.
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