Chemical apparatus; Electroplating; Glass blowing and working; Glass coatings; Glass grinding and polishing; Lampwork; Mirrors
By pumping and sparking, the resistance of the tube may be gradually
raised till the spark would rather jump over 2 inches of air than go
through the tube. When this state is attained the Roentgen effect as
tested by a screen of calcium tungstate should be very brilliant. No
conclusion as to the equivalent resistance of the tube can be arrived
at so long as the discharge is kept going continually. When the spark
would rather go over an inch of air in the spark gap than through the
tube the pumping and sparking may be interrupted and the tube allowed
to rest for, say, five minutes. It will generally be found that the
equivalent resistance of the tube will be largely increased by this
period of quiescence. It may even be found that the spark will now
prefer to pass an air gap 3 inches long.
In any case the sparking should now be continued, the pump being at
rest, and the variations of tube resistance watched by adjusting the
spark gap. If the resistance falls below an equivalent of 2 inches of
air in the gap the pump must be brought into action again and
continued until the resistance as thus estimated remains fairly
constant for, say, ten minutes. When this occurs the narrow neck of
the exhaust tube may be strongly heated till the blow-pipe flame
begins to show traces of sodium light. The flame must then be
withdrawn and the discharge again tested. This is necessary because
it occasionally happens that gas is given off during the heating of
the neck to the neighbourhood of its fusion temperature.
If all is right the neck may now be fused entirely off and the tube is
finished. Tubes of the focus pattern with large platinum anodes are
in general (in my experience) much more difficult to exhaust than
tubes of the kind first described. This is possibly to be attributed
mainly to the gas given off by the platinum, but is also, no doubt,
due to the tubes being much larger and exposing a larger glass
surface. The type of tube described first generally takes about two
hours to exhaust by a pump made as explained, while a "focus" tube has
taken as long as nine hours, eight of which have been consumed after
the tube was exhausted to the hammering point.
Public-domain text, read in full here on John Shaqi.
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