Perfumes and their preparation : $b Containing complete directions for making handkerchief perfumes, smelling-salts, sachets, fumigating pastils; preparations for the care of the skin, the mouth, the hair; cosmetics, hair dyes, and other toilet articlesAskinson, George William
Science
Perfumes and their preparation : $b Containing complete directions for making handkerchief perfumes, smelling-salts, sachets, fumigating pastils; preparations for the care of the skin, the mouth, the hair; cosmetics, hair dyes, and other toilet articles
Askinson, George William
Cosmetics; Perfumes
When working with an open fire, as soon as vapors appear at the lower
end of the worm (Fig. 9), cold water is admitted through the tube _ne_;
as the cold water abstracts heat from the vapors and condenses them, it
becomes warm, rises to the surface, and escapes through _b_, so that
the worm is continually surrounded with cold water. If for any reason
the saving of cold water is an object, its flow may be so regulated
that the vapors are just condensed, the warm distillate being allowed
to cool in the air. When working with steam, the cold water must be
admitted the moment the steam-cock is opened, and the flow of cold
water should be ample during the distillation, which in this case is
much shorter.
The large apparatuses here described are generally used, especially
for the extraction from vegetable substances of odors present in
considerable quantity, for instance, mace, nutmeg, cloves, cinnamon,
etc., or from bulky material as the various flowers. For very expensive
odors, smaller apparatuses are often employed, the construction of
which resembles that of the ones described. For this purpose small
glass apparatuses are very suitable; they are illustrated in Fig. 12.
The still, a retort A, consists of a spherical vessel with a bottle
neck _t_ which is either closed with a cork or carries a thermometer
or glass tube, and with a lateral tube, the neck of the retort,
connected with the adapter _r_. The latter passes into the condenser
C. At the lower end of R is the bent adapter _v_ under which is placed
the receptacle for the distillate. The tube C is closed with corks,
at its lower end is the ascending tube _h_, and at its upper end the
descending tube _g_. During the distillation cold water flows in
through _h_ which cools the tube _r_ and escapes at _g_. The tube C,
as will be readily understood, acts like the condenser in the larger
apparatuses above described. In order to prevent the breaking of the
retort, it is not heated over a flame, but is set in a tin vessel B
filled with water. The comminuted vegetable material is inserted with
water through the up-turned neck of the retort into the latter; the
vessel B is filled with water which is raised to the boiling-point.
[Illustration: FIG. 12.]
During distillation we obtain at the lower end of the condenser pure
water and essential oil. When larger quantities are to be distilled
it is advisable to use a Florentine flask as a receptacle for the
separation of the oil and water (Fig. 13). It consists of a glass
bottle from the bottom of which ascends a tube curved above; the latter
rises high enough to bring the curvature slightly below the neck of the
flask. During the distillation the flask becomes filled with water W,
on which floats a layer of oil O; the excess of water escapes through
_a_ at _d_ until the flask finally contains more oil and very little
water.
[Illustration: FIG. 13.]
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