Perfumes and their preparation : $b Containing complete directions for making handkerchief perfumes, smelling-salts, sachets, fumigating pastils; preparations for the care of the skin, the mouth, the hair; cosmetics, hair dyes, and other toilet articlesAskinson, George William
Science
Perfumes and their preparation : $b Containing complete directions for making handkerchief perfumes, smelling-salts, sachets, fumigating pastils; preparations for the care of the skin, the mouth, the hair; cosmetics, hair dyes, and other toilet articles
Askinson, George William
Cosmetics; Perfumes
When producing essential oils on a large scale, instead of the frail
Florentine flasks it is advisable to use separators, the construction
of which is illustrated in Fig. 14. They consist of glass cylinders,
conical above and below, supported on a suitable frame. The water
accumulating under the oil is allowed to escape by opening the
stop-cock; when the first separator is filled with oil, the succeeding
distillate passes through the horizontal tube into the next separator,
etc.
[Illustration: FIG. 14.]
When the distillation is carried on in an ordinary still, we obtain,
besides the essential oil, a considerable quantity of aromatic water,
that is, a solution of the oil in water.
An apparatus which obviates the losses caused thereby is that of
Schimmel described below, which is well adapted to the manufacture on a
large scale. The apparatus is patented.
The nearly spherical still D (Fig. 15) is surrounded by a jacket M;
the inlet steam tube R is connected with a branch _r_ which enters the
interior of the still as a spiral tube with numerous perforations,
while R opens into the space M. When _r_ is opened, distillation takes
place by direct steam; when R is opened, by indirect steam; when both
faucets are opened, the still is heated at the same time with direct
and indirect steam.
[Illustration: FIG. 15.]
The vapors rising from the still D pass through the helm C and the tube
A into the worm K; the fluid condensed in the latter drops into the tin
Florentine flask F, the aromatic water flowing from the latter passes
back into the still D through the Welter funnel T and is distilled over
again, so that the entire distillation can be effected with very little
water, and it is continued until the water escaping from the Florentine
flask is freed from oil and odorless.
When working with superheated steam, it is necessary to set under the
funnel tube T a vessel twice the size of the Florentine flask, which is
provided with a stop-cock above and below. The lower cock is closed,
the vessel is allowed to fill with water from F, then the upper cock is
closed, the contents being allowed to escape into D by opening, when
the cocks are again reversed.
The use of superheated steam is important especially with material
which gives up the contained oil with difficulty, such as woods.
[Illustration: FIG. 16.]
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