Petroleum; Petroleum -- Great Britain; Petroleum engineering
The steam and ammonia gas liberated in the still pass over into a
large lead-lined tub or saturator, and bubbles through holes in a
lead worm placed round the circumference at the bottom of the vessel.
Sulphuric acid is at the same time run into the saturator, and, at
a certain temperature, sulphate of ammonia is formed. The sulphate
falls into a well, formed in the centre of the bottom of the vessel,
in which are placed two steam ejectors, and these blow it out along
with some liquor. This mixture is delivered into hutches having
perforated bottoms, through which the ammonia liquor drains off, the
solid sulphate being left in the hutch. This is now run by an overhead
railway to the drying or storage stalls, and from these it is packed
up and dispatched to the market. The exhaust steam and waste gases
from the saturator are passed into the retorts, and utilized for the
formation of ammonia from the shale, while the spent water is pumped to
the spent shale bing, and thoroughly filtered before being allowed to
escape from the works.
For dealing with the weak acid water recovered from the refinery, the
Pumpherston plant consists of lead-lined tubs or crackers, into which
a quantity of the acid water is run, and saturated with ammonia gas
until it is near the salting point, when it gravitates into settling
vessels in order to separate any tar carried over with the acid water.
The clear liquid is then drawn into the saturator, where it is quickly
converted into sulphate and blown out in the manner already described.
So up to date is the whole of the system governing the treatment of the
shales and the resulting products, that the pumping of water from the
mines, the haulage of the shale to the refineries, as well as driving
of machinery in the works, is performed by electric power, the exhaust
steam from the engines driving the generators, as in the case of the
sulphate of ammonia exhaust, being sent to the retorts for use in the
production of ammonia.
The process of refining the crude oil obtained from the shale into
the various products is somewhat complicated and perplexing to those
unassociated with the industry on account of the many distillations
and treatments which have to be carried out before a good marketable
article is produced. The following outline, however, will give a fair
idea of the process adopted throughout Scotland.
Public-domain text, read in full here on John Shaqi.
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