=149. Accuracy of Results.=—A sample of soil from the beet sugar
station, in Nebraska, gave the following duplicate results:
First trial 45.75 per cent water.
Second trial 44.85 „ „ „
Muck soils from Florida, containing varying proportions of sand, gave
the following numbers:
Soil number one, 144.85 per cent, and 145.43 per cent; soil number
two, 109.13 per cent, and 107.93 per cent; soil number three (very
sandy), 46.86 per cent, and 46.51 per cent.
=150. Method of Wollny.=[105]—A zinc tube, ninety centimeters long and
four centimeters internal diameter, carries at each end, at right angles
to the axis, a flattened rim 1.5 centimeters broad. The lower end of the
tube is closed with a strong piece of coarse linen. The soil to be
examined is then filled in little by little, with gentle tamping.
On the upper end two glass tubes are placed, each ten centimeters long
and four centimeters internal diameter. These tubes are furnished at
each end with cemented brass cylinders which are expanded to a circular,
evenly ground rim, 1.5 centimeters wide, also at right angles to the
axis of the main tube. These rims are greased and placed together, one
on the other, and held together by wooden clamps.
The glass tube in immediate connection with the zinc tube is also firmly
filled with the soil sample, while the second tube is only partly
filled, so that any settling which may take place in the soil on the
addition of water may still find the first glass tube full of the
sample.
The empty part of the upper glass tube is now filled with water and
additional quantities of water are added from time to time until the
soil is saturated. In order to be able to observe when this takes place
there is a slit at the lower end of the zinc tube which is closed with a
piece of glass. This slit should be about two centimeters broad and ten
centimeters long. The lower end of the zinc tube is set on a glass plate
to prevent evaporation.
As soon as the water shows itself at the lower end of the zinc tube, the
excess of water in the upper glass tube is at once removed by a pipette
and a stopper inserted through which a glass tube passes drawn out into
a fine point above. The object of this is to avoid evaporation on the
upper surface. The apparatus is then left at rest for thirty-six hours.
At the end of this time the clamps are removed and the column of moist
earth cut with a piece of platinum foil, and the two ends of the glass
tube, next to the zinc tube, covered with glass plates. It is then
weighed and the weight of moist earth determined by deducting the weight
of the tube and its glass covers. The moist earth is carefully removed
to a large porcelain dish and dried at 100°. Before weighing it is
allowed to stand twenty-four hours in the air. The data obtained are
used to calculate the water content to volume per cent.
The volume of the glass tubes should be determined by careful
calibration.
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