In practice the use of cylindrical apparatus with or without mechanical
stirring and the method by decantation have proved to be the most
reliable and satisfactory procedures. Between the beaker and churn
methods, of separation there is little choice in regard to accuracy.
Which is the superior method, is a question on which the opinions of
experienced analysts are divided. The various processes will be
described in the order already mentioned.
=198. Methods Depending on Subsidence of Soil Particles.=—The simplest
method of effecting the further separation of the soil particles is
without doubt that process which permits them to fall freely in a liquid
sensibly at rest. The practical difficulties of this method consist in
the trouble of securing a perfect separation of the particles, in
preventing flocculation after division and in avoiding currents in the
liquid of separation.
For the separation of the soil particles for this method boiling and wet
pestling are the only means employed. The flocculation of the separated
particles may be partially prevented by adding a little ammonia to the
water employed. The author has also tried dilute alcohol as the
separating liquid but the results of this method are not yet
sufficiently definite to find a place in this manual. Evidently the
practical impossibility of avoiding convection currents prevents the use
of water at a high temperature for this separation, although the
tendency to flocculation almost disappears as the temperature approaches
100°. The general method of avoiding the errors due to flocculation in
the subsidence method consists in repestling the deposited particles and
thus subjecting them as often as may be necessary to resedimentation.
These principles are well set forth by Osborne,[133] who states that
when a soil is completely suspended in water by vigorous agitation,
particles of all the sizes present are to be found throughout the entire
mass of liquid. When subsidence takes place, the larger particles will
go down more rapidly than the smaller ones, but some of the small
particles that are near the bottom will be deposited sooner than some of
the larger ones which have a much greater distance to travel. Thus,
independently of the fact that the larger particles in their descent are
somewhat impeded by the smaller, the smaller being at the same time
somewhat hastened by the larger, the sediment that reaches the bottom at
any moment is a more or less complex mixture of all the mechanical
elements of the soil. The liquid, however, above this sediment at the
same moment will have completely deposited all particles exceeding
certain dimensions of hydraulic value, determined mainly by the time of
subsidence.
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