With another sieve having spaces of one millimeter, the coarse sand is
separated. The pebbles and sand are dried, weighed, treated with
hydrochloric acid and again weighed in order to find the quantity of
calcareous matter contained in them. In ten grams of this fine earth the
humidity is determined by drying at 100°.
Ten grams are mixed in a capsule with fifteen to twenty cubic
centimeters of water and after eight to ten seconds the supernatant
liquid is poured into a beaker having a capacity of 250 cubic
centimeters. The same operation is repeated until there are contained in
the beaker the fine sand and the clay, while the coarser sand remains in
the capsule.
This last is then dried and weighed and the quantity of calcium
carbonate determined by treating it with diluted nitric acid. By means
of calcination the organic matter is determined. The liquid decanted in
the beaker, the volume of which must not surpass 200 to 250 cubic
centimeters, is treated with nitric acid, filtered after some time,
washed and the calcium is directly determined by precipitating the
solution with ammonium oxalate.
The part in the filter which contains the fine sand, the clay, and the
humus material is mixed with water to a volume of about 200 cubic
centimeters; there are then added to it two to three cubic centimeters
of ammonia and after two or three hours it is diluted to a liter and
strongly agitated.
After twenty-four hours of rest it is decanted and the residuum is
treated a second time with diluted ammonia, decanting after twenty-four
hours. Ordinarily these two treatments suffice, if, however, the earth
is very argillaceous, this operation should be repeated three and even
four times.
The clay which is found in the liquid suspended in colloidal form
coagulates and is precipitated by adding thirty to forty cubic
centimeters of a saturated solution of potassium chlorid, while the
humus substance, under the influence of the ammonia remains dissolved.
Sestini found that the method of Schloesing was the only one which
indicated exactly the quantity of clay in the soil. He modified this
method by reducing the time of rest from twenty-four hours, as proposed
by Schloesing, to only twelve hours, a reduction which in his opinion
does not in the least impair the exactness of the method.
Sestini also proposes twelve treatments instead of six.
SEPARATION OF THE SOIL PARTICLES BY A LIQUID IN MOTION.
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