Holthof modifies the apparatus of Schöne by putting into the lower mouth
of the elutriator a little mercury so that the particles of earth are
deposited upon its surface and are thus better agitated and washed by
the current of water.
=218. Mayer’s Modification of Schöne’s Method.=—An improvement of
Schöne’s apparatus in the direction of greater simplicity has been
tested by Mayer[150] with satisfactory results:
The apparatus, (Fig. 34), consists of a glass vessel having a glass
stop-cock at the bottom for admitting the water. For a distance of
twenty centimeters the sides of the tube are parallel and the diameter
about one centimeter. Next for a distance of fifty centimeters the tube
is conical expanding at a regular rate until the internal diameter
reaches five centimeters. For a distance of ten centimeters the vessel
is again strictly cylindrical and it is in this cylindrical portion that
the separation of the different constituents takes place. The vessel is
then rapidly narrowed until it carries the stopper A two centimeters in
diameter. This stopper carries two glass tubes, one F bent downward to
conduct the overflow into the receiving vessels, and one H for the
purpose of regulating the rate of overflow by the height of the column
of water therein. The orifice of the overflow tube F should be so
regulated that with a pressure of five centimeters water in H, one liter
shall pass over in ten minutes.
[Illustration:
FIGURE 34.
SCHÖNE’S APPARATUS
FOR SILT
ANALYSIS,
MODIFIED
BY MAYER.
]
If the separation be conducted in an apparatus thus mounted and
graduated with a pressure of two centimeters in H all that portion of
the soil which can properly be called clay will pass over. The fine
earth, that is, earth in which all coarse particles have been removed by
proper sifting, is used in ten-gram lots for each experiment. The
residue, after the separation is complete, consists of pure sand or at
least pure sand mixed with humus. Before the fine earth is placed in the
apparatus, the calcium carbonate therein is removed with hydrochloric
acid. The treatment with hydrochloric acid, however, is not to be
recommended in soil containing many undecomposed particles of calcium
carbonate or dolomite for then large additions to the silt output might
be made from these particles, which could not be regarded as coming from
the soil as it actually exists. For alluvial soil, however, previous
treatment with hydrochloric acid is recommended unconditionally.
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