It is desirable to run off the upper third of the column at intervals of
fifteen to twenty minutes by temporarily increasing the velocity. Recent
sediments, river alluvium, etc., are more easily separated than soils of
more ancient formation. The second, third, etc., separations are
naturally accomplished in much less time than the first. The respective
velocities of the separations should be 0.25 millimeter, 0.50
millimeter, one millimeter, two millimeters, four millimeters, eight
millimeters, sixteen millimeters, thirty-two millimeters, and sixty-four
millimeters a second. Below a velocity of four millimeters a second the
mechanical stirrer is indispensable. Above this velocity the current of
water in the conical base will be sufficient to bring the desired
particles into the ascending column. At this velocity also a smaller
elutriating tube having one-half or one-quarter the cross-section of the
first may be employed to hasten the operation and diminish the quantity
of water required. The quantity of water required for a complete
separation is from 100 to 120 liters. Any soft water free of organic
matter may be used, but distilled water is best. Hard water should be
avoided.
The mean time required for the different separations is as follows: 0.25
millimeter hydraulic value, thirty-five hours; 0.50 millimeter hydraulic
value, twenty hours; one millimeter hydraulic value, seven and a half
hours; two to sixty-four millimeters hydraulic value, eight hours. With
proper arrangements for night work, an analysis may be finished in three
or four days not counting the time required for the previous separation
of the clay.
=231. Weighing the Sediments.=—The sediments should be dried at the same
temperature used for drying the soils. Hilgard dries both at 100°. Great
care should be used in weighing the exceedingly hygroscopic clay
sediments. In the case of the sediment of 0.25 millimeter hydraulic
value it is allowed to subside as much as possible and after removing
the supernatant water the residue, twenty-five to fifty cubic
centimeters, is evaporated in a platinum dish and weighed therein. The
water can be completely decanted from the other sediments, and they can
be dried and weighed without any unusual precautions.
The loss in the separation of clays and subsoils containing but little
organic matter is usually from 1.5 to 2 per cent. This loss is partly
due to the fine silt which comes off during the whole of the process and
which is lost in the decanted waters of the sediments of 0.25
millimeters hydraulic value and above. The procedures indicated above
are not strictly applicable to soils rich in humus and other organic
matters, but the destruction of these matters by ignition leaves the
residual soil in a condition wholly unfit for sedimentary separation.
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