The staining of the particles after ignition and treatment with acids
gives better results than the direct treatment. Particles of carbonate
which are stained with difficulty before ignition take the stain easily
afterwards on account of the decomposition produced by the loss of
carbon dioxid. This is the case also with particles containing water of
composition or crystallization.
=257. Cleavage of Soil Particles.=—A microscopic examination of the
cleavage of soil particles may be useful in determining their mineral
origin. The course followed by cleavage lines and their mutual position
is dependent on the direction in which the separation of the mineral
fragment takes place. The character of the microscopic fragments
produced by crushing a soil particle is determined primarily by the
system of crystallization to which it belongs. Perhaps the most
distinguishing cleavage marks in soil particles will be found in
fragments of mica and orthoclase. These characteristic forms are shown
in Figs. 39 and 40. The first (Fig. 39) shows the pinacoidal cleavage in
a fragment of mica. Fig. 40 illustrates the appearance of the cleavage
lines in a fragment of orthoclase. Figs. 41 and 42 show the
characteristic cleavage lines in fragments of epidote and titanite.
=258. Microchemical Examination of Silt.=—The methods of quantitative
chemical examination of silts will be given in another part of this
manual. Certain qualitative and microchemical tests, however, are useful
in identifying silt particles. For instance, any soluble iron mineral
will be detected, even in minute quantity, by the blue coloration of the
solution produced by the addition of potassium ferrocyanid. Manganese
will be revealed by fusion with soda and saltpeter on platinum foil, in
the oxidizing flame, producing the well-known green coloration due to
the sodium manganate formed.
More valuable indications of the character of the fragments examined are
obtained by microchemical processes. The best method of decomposing the
silt particles for this purpose is by treatment with hydrofluosilicic
acid. When the particles are composed of silicates, pure hydrofluoric
acid is to be preferred.
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