In the apparatus of Harada,[176] Fig. 59, the separating vessel _a_ is
made of thick glass furnished with a glass stopper above and a glass
stop-cock _h_ below. The separating liquid and silt are placed in the
pear-shaped vessel _a_, the stopper inserted, and the whole well-shaken.
As soon as a ring of clear liquid is seen between the sinking and
floating silt, the lower end of the apparatus is brought near the bottom
of a conical glass _b_, the cock _h_ opened and the heavy silt allowed
to fall out. Very little of the liquor will flow out because of the air
pressure. Should an air bubble enter the apparatus and be held at the
stop-cock, it should be made to ascend by gently tapping. When all the
heavy silt has passed into the conical glass, the cock _h_ is closed and
some water poured over the solution and silt in _b_. The separatory
apparatus is now raised until the beveled end of it is in the water
layer, when the water at once rises to _h_ and thus washes all the silt
particles adhering to the glass into _b_. The liquid in _a_ may then be
diluted by inverting the apparatus, adding the required amount of water
through _h_, again shaken after closing _h_, and another separation
secured as before.
This apparatus is somewhat easier to manipulate than Thoulet’s but does
not admit of the same quantitative dilution of the separating liquid.
[Illustration:
FIG. 60 a. FIG. 60 b. FIG. 60 c.
BRÖGGER’S APPARATUS.
]
=271. Apparatus of Brögger.=—All silt separations in narrow tubes are
open to the objection of permitting more or less flocculation. Some of
the lighter particles are thus carried down by the heavier, and, on the
other hand, some of the heavier float with the lighter. This disturbing
action Brögger[177] seeks to avoid by the following device, Fig. 60, a,
b, c. The length of the apparatus is forty-six centimeters, and its
greatest diameter 3.5 centimeters. The opening in the large stop-cock A
is the same diameter as that of the apparatus at that point. The cubical
content of the apparatus with A open and B closed is about seventy-five
cubic centimeters. In conducting the separation the cock B is closed,
the separating liquid and silt introduced, A being open, the stopper K
inserted and the whole well-shaken. In the first separation, the silt S,
lying over B is contaminated with some of the lighter particles S′₂,
while the lighter particles above A, S₂, are mixed with some of the
heavier particles, S′₁. After closing A the apparatus is again
well-shaken and inverted as in Fig. 60 b. The two parts of the silt will
now undergo another separation as indicated. The apparatus is now
carefully inclined as in c, when the various grades of silt will flow in
the directions indicated by the arrows, but without mixing, passing each
other on opposite sides of the apparatus. When the movement is complete,
A is carefully opened, the apparatus still being held as in c, and the
light silt formerly between A and B will flow above A, while the heavy
Public-domain text, read in full here on John Shaqi.
Reviews
Reviews
No reviews yet
Be the first to share your thoughts on this work.
Elsewhere in the archive
Join the Discussion
Join the discussion
Sign in to leave a comment or review.
Sign InorCreate an account