Pulverize the air-dried soil in a mortar with a wooden pestle, and
separate the fine earth by a sieve with meshes three millimeters wide;
this sieve should have a tightly fitting cover of sheepskin stretched
over a loop, and it should be covered in the same manner underneath, so
that no dust can escape during the process of sifting.
Wash the pebbles and vegetable fibers remaining on the sieve with water,
dry and weigh the residue; the water with which this gravel was washed
should be evaporated to dryness at a temperature not exceeding 50°
towards the close of the evaporation, and the residue mixed with what
passed through the dry sieve.
The sifted fine earth is reserved for all the processes hereinafter
described, and is kept in well-stoppered bottles, marked air-dried fine
earth. The sieve mentioned above is too coarse for the more modern
methods of analysis.
=83. Wolff=[64] directs that the air-dried earth (in summer dried in
thin layers at room temperature, in winter in ovens at 30° to 50°) be
freed from all stones, the latter washed, dried, and weighed. The soil
is next passed through a three millimeter mesh sieve, the residual
pebbles and fiber washed, dried and weighed. The fine earth passing the
sieve is used for all subsequent examinations. It is air-dried at
moderate temperatures and preserved in stoppered glass vessels.
=84. The French=[65] commission calls especial attention to the method
of subsampling, and prescribes that the sample of earth which has been
taken in the manner indicated, and of which the weight should be greater
as the material is less homogeneous should not be analyzed as a whole.
It should be divided into two parts. The first includes the finer
particles constituting the earth, properly so-called, with the elements
which alone enter into play in vegetable nutrition and on which it is
necessary to carry out the analysis. The second embraces the coarser
particles to which only a superficial examination should be given and
which may have a certain importance from a physical point of view but
which cannot take any part from a chemical point of view, in the
nutrition of plants. It is, however, useful to examine its mineralogical
constitution and to look for the useful elements such as lime, potash,
etc., which it may be able to furnish to the earth, and in proportion as
it is decomposed, finer particles which may be useful in plant
nutrition.
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