The calorimeter is shown in the figures B and B′. It consists of a
wooden box closed on one side by a glass plate G and on the other to the
heighth F by a small board on which a calorimeter of ordinary
construction is placed. The cylinder of the calorimeter is seventy
millimeters high and forty-seven millimeters in diameter.
[Illustration:
FIGURE 13.
REGNAULT’S APPARATUS FOR DETERMINING THE SPECIFIC HEAT OF SOILS.
]
This part of the apparatus is supported by triangular pieces of cork. A
delicate thermometer is fastened to the top of the box of the
calorimeter and the value of the degrees is so arranged that about
twelve of them correspond to about one degree C. The scale of the
instrument can be arbitrarily fixed and the temperature of any part of
it determined by comparison with a delicately graduated thermometer.
Near the thermometer in the calorimeter is a stirrer made of a very thin
copper disk with a bent rim. This stirrer is operated by means of a silk
cord moved by appropriate machinery.
The reading of the thermometer is made through a glass plate and this
should be protected from the heat of the body of the observer by a paper
screen.
The test tube E is first filled with the substance, whose specific heat
is to be determined, and weighed. It is then placed in the water bath
until constant weight is reached. After constant weight has been
obtained the apparatus is again dried and the exact weight of the
moisture lost thus determined. The test tube is then placed in the
apparatus A closed with a well-fitted cork, the top covered with cotton
and heated in the aqueous vapor for about one hour. The heating
apparatus should be far removed from the calorimeter so that the
temperature of the latter cannot be influenced thereby. Meanwhile the
calorimeter is filled with water which has stood in the room for a long
time until it has acquired, as nearly as possible, the room temperature.
The quantity of water is such that the water value of the whole of the
calorimeter together with the immersed portions of the thermometer and
stirrer shall amount to exactly 100 grams. A few minutes before bringing
the substance into the calorimeter, the stirring apparatus is put in
motion and the temperature observations are commenced. These should be
at intervals of twenty seconds and should be continued until ten
observations have been made. Meanwhile the height of the barometer is
also read. A few seconds before the tenth interval the apparatus A is
brought quickly to the calorimeter and its contents emptied into it at
the moment of the tenth interval. The apparatus A should be removed as
quickly as possible after its contents are emptied.
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