Double the quantity of the beet pulp required for the ventzke
polariscope, _viz._, 52.096 grams, weighed in a lipped metal dish,
is washed, by means of alcohol, into a flask marked at 202.6 cubic
centimeters, and the flask filled two-thirds with ninety-five per
cent alcohol and well shaken. Afterwards, a proper quantity of lead
subacetate is added, and then sufficient alcohol to complete the volume
to the mark. The flask is then attached to the condenser, placed in
a water-glycerol bath and heated to a temperature of 75° for about
forty-five minutes. At the end of this time, the flask is removed from
the bath and condenser, cooled quickly with water, alcohol added to
the mark and well shaken. The filtration should be accomplished with
precautions, to avoid the loss of alcohol mentioned in paragraph =221=.
The filtrate is examined in the polariscope in a 200 millimeter tube,
and the reading obtained gives directly the percentage of sugar in the
sample examined. Half the quantity of pulp mentioned, in a 101.3 cubic
centimeter flask, may also be used. A convenient form of arranging a
battery of flasks is shown in the accompanying figure.
[Illustration: FIG. 71. BATTERY FOR ALCOHOLIC DIGESTION.]
=224. Determination of Sugar in Mother Beets.=—In selecting mother
beets for seed production, it is necessary to secure only those of a
high sugar content. This is accomplished by boring a hole about two and
a half centimeters in diameter obliquely through the beet by means of
the apparatus shown in Fig. 72.
The beet is not injured for seed production by this process, and the
pulp obtained is used for the determination of sugar. The juice is
expressed by means of the small hand press shown in Fig. 73. Since only
a small quantity of juice is obtained, it is advisable to prepare it
for polarization in a sugar flask marked at fifty cubic centimeters.
The density of the juice, by reason of its small volume, is easiest
obtained by the hydrostatic balance, as described in paragraph =53=.
In lieu of this, the juice may be quickly weighed in a counterbalanced
dish on a balance giving results accurate to within one milligram. The
rest of the analytical process is similar to that already described.
[Illustration: FIG. 72. RASP FOR SAMPLING MOTHER BEETS.]
[Illustration: FIG. 73. HAND PRESS FOR BEET ANALYSIS.]
[Illustration: FIG. 74.]
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