=226. Determination of Sugars without Weighing.=—An ingenious device
for the rapid analysis of mother beets is based upon the use of a
machine which cuts from the beet a core of given dimensions and this
core is subsequently reduced to a pulp which is treated with cold water
and polarized in the manner described above. The cutting knives of the
sampler can be adjusted to take a core of any desired size. Since the
beets used for analysis have essentially the same specific gravity, the
cores thus taken weigh sensibly the same and the whole core is used
for the analysis, thus doing away with the necessity of weighing. The
core obtained is reduced to a pulp in a small machine so adjusted as
to permit the whole of the pulp, when prepared, to be washed directly
into the sugar flask. By the use of this machine a very large number of
analyses can be made in a single day, and this is highly important in
the selection of mother beets, for often 50,000 or 100,000 analyses are
to be made in a short time.
[Illustration: FIG. 75. TUBE FOR CONTINUOUS OBSERVATION.]
=227. Continuous Diffusion Tube.=—To avoid the delay occasioned by
filling and emptying observation tubes in polariscopic work, where
large numbers of analyses of canes and beets are to be made, Pellet
has devised a continuous diffusion tube, by means of which a solution,
which has just been observed, is rapidly and completely displaced by a
fresh solution. This tube, improved by Spencer, is shown in Fig. 75.
The fresh solution is poured in at the funnel, displacing completely
the old solution which flows out through the tube at the other end.
The observer watches the field vision and is able to tell when the
old solution is completely displaced by the clearing of the field, at
which time the reading of the new solution can be quickly made. When
solutions are all ready for examination an expert observer can easily
read, by the aid of this device, from four to five of them in a minute.
=228. Analysis of Sirups and Massecuites.=—The general principles which
control the analysis of sirups and massecuites are the same whether
these products be derived from canes or beets. In the case of the
products of canes, the sirups or massecuites contain chiefly sucrose,
invert sugar, and other copper reducing bodies, inorganic matters and
water. In the case of products derived from sugar beets the contents
are chiefly sucrose, inorganic matters, a trace of invert sugar,
raffinose and water. The principles of the determination of these
various constituents have already been described.
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