From vegetable substances, such as seeds, the fat is extracted either
by pressure or by the use of solvents. For quantitive purposes, only
solvents are employed. The dry, finely ground material is exhausted
with anhydrous ether or petroleum spirit, in one of the convenient
forms of apparatus already described (=33->43=). In very oily seeds
great difficulty is experienced in securing a fine state of subdivision
suited to complete extraction. In such cases it is advisable to conduct
the process in two stages. In the first stage the material, in coarse
powder, is exhausted as far as possible and the percentage of oil
determined. The residue is then easily reduced to a fine powder, in an
aliquot part of which the remaining oil is determined in the usual way.
[Illustration: FIG. 79.—OIL PRESS.]
In securing oils for physical and chemical examination both pressure
and solution may be employed. The purest oils are secured by pressure
at a low temperature. To obtain anything like a good extraction some
sort of hydraulic pressure must be used. In this laboratory a press
is employed in which the first pressure is secured by a screw and
this is supplemented by hydraulic pressure in which glycerol is the
transmitting liquid. The construction of the press is shown in the
accompanying figure.
The whole press is warmed to nearly 100°. The hot finely ground oily
material, enclosed in a cloth bag, is placed in the perforated cylinder
and compressed as firmly as possible by turning with the hands the
wheel shown at the top of the figure. The final pressure is secured by
the screw shown at the bottom of the figure whereby a piston is driven
into a cylinder containing glycerol. The degree of pressure obtained is
equal to 300 atmospheres.
Even with the best laboratory hydraulic pressure not more than
two-thirds of the total oil contents of oleaginous seeds can be secured
and the process is totally inapplicable to securing the oil from
tissues when it exists in quantities of less than ten per cent. To get
practically all of the oil the best method is to extract with carefully
distilled petroleum of low boiling point.
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