0° 0.999871 21° 0.998047
1° 0.999928 22° 0.997826
2° 0.999969 23° 0.997601
3° 0.999991 24° 0.997367
4° 1.000000 25° 0.997120
5° 0.999990 26° 0.996866
6° 0.999970 27° 0.996603
7° 0.999933 28° 0.998331
8° 0.999886 29° 0.995051
9° 0.999824 30° 0.995765
10° 0.999747 31° 0.995401
11° 0.999655 32° 0.995087
12° 0.999549 33° 0.994765
13° 0.999430 34° 0.994436
14° 0.999299 35° 0.994098
15° 0.999160 36° 0.993720
16° 0.999002 37° 0.993370
17° 0.998841 38° 0.993030
18° 0.998654 39° 0.992680
19° 0.998460 40° 0.992330
20° 0.998259
From the table and the weight of water found, the volume of the
pyknometer is easily calculated.
_Example._—Let the weight of water found be 11.72892 grams, and the
temperature 20°. Then the volume of the flask is equal to 11.72892 ÷
0.998259, _viz._, 11.95 cubic centimeters.
=50. Use of Pyknometer at High Temperatures.=—It is often found
desirable to determine the density of a liquid at temperatures above
that of the laboratory, _e. g._, at the boiling-point of water. This is
easily accomplished by following the directions given below:
_Weight of Flask._—Use a small pyknometer of from twenty-five to thirty
cubic centimeters capacity. The stopper should be beveled to a fine
edge on top and the lower end should be slightly concave to avoid any
trapping of air. The flask is to be thoroughly washed with hot water,
alcohol and ether, and then dried for some time at 100°. After cooling
in a desiccator the weight of the flask and stopper is accurately
determined.[27]
[Illustration: FIGURE 28. BATH FOR PYKNOMETERS.]
_Weight of Water._—The flask in an appropriate holder, Fig. 28,
conveniently made of galvanized iron, is filled with freshly boiled and
hot distilled water and placed in a bath of pure, very hot distilled
water, in such a way that it is entirely surrounded by the liquid with
the exception of the top.
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