Next to the compensating apparatus is the analyzing nicol which in
this instrument is fixed in a certain place, _viz._, the zero of the
scale. The analyzer and the telescope for observing the field of vision
are carried in the tube HJ. The movable quartz wedge has a scale which
is read with a telescope K, provided with a mirror inclined at an angle
of 45°, just over the scale and serving to illuminate it. The quartz
wedges are also provided with a movement by which the zero point of
the scale can be adjusted. A kerosene lamp with two flat wicks is the
best source of illumination and the instrument should be used in a dark
room and the light of the lamp, save that which passes through the
polariscope, be suppressed by a shade. The sensitive or transition tint
is produced by that position of the regulating apparatus which gives
a field of view of such a nature that a given small movement of the
quartz compensating wedge gives the greatest contrast in color between
the halves of the field of vision. For most eyes a faint rose-purple
tint, as nearly colorless as possible, possesses this quality. A slight
movement of the quartz wedge by means of the screw head M will, with
this tint, produce on one side a faint green and on the other a pink
color, which are in strong contrast. The neutral point is reached by so
adjusting the quartz wedge as to give to both halves of the field the
same faint rose-purple tint.
=74. The Shadow Polariscope for Lamp Light.=—This form of instrument
is now in general use for saccharimetric purposes. It possesses on
the one hand, the advantages of those instruments using monochromatic
light, and on the other, the ease of manipulation possessed by the tint
polariscopes. It differs from the tint instrument in dispensing with
the nicol and quartz plate used to regulate the sensitive tint, and
in having its polarizing nicol peculiarly constructed in harmony with
the optical principles of the jellet-corny prism. The more improved
forms of the apparatus have a double quartz wedge compensation. The
two wedges are of opposite optical properties, and serve to make
the observations more accurate by mutual correction. The optical
arrangement of the different parts of such a polariscope is shown in
the following figure.
The lenses for concentrating the rays of light and rendering them
parallel are contained in the tube N. At O is placed the modified
polarizing nicol. The two compensating quartz wedges are moved by the
milled screw-heads EG. The rest of the optical apparatus is arranged
as described under the tint polariscope. For practical purposes, only
one of the wedges is employed, but for all accurate work the readings
should be made with both wedges and thus every possible source of error
eliminated.
[Illustration: FIGURE 38. DOUBLE COMPENSATING SHADOW POLARISCOPE.]
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