Pyrometry: A Practical Treatise on the Measurement of High Temperatures — John Shaqi
Pyrometry: A Practical Treatise on the Measurement of High TemperaturesDarling, Charles R. (Charles Robert)
Science
Pyrometry: A Practical Treatise on the Measurement of High Temperatures
Darling, Charles R. (Charles Robert)
Pyrometry
=Management of Thermo-electric Pyrometers.=—Generally speaking,
thermo-electric pyrometers give little trouble in practice, but the
management should always be placed in skilled hands. It is advisable
to test each instrument periodically at a fixed point near the working
temperature, by the method explained on page 57; and if two or three
pounds of material be used, the protecting shield need not be removed.
A useful material for checking pyrometers near the critical range of
steel is an alloy of 60 per cent. of copper and 40 per cent. of tin,
which gives a well-defined freezing point at 738° C., and which may be
used indefinitely in a reducing atmosphere Any serious error is easily
detected by observing that the indications differ widely from those
generally obtained under the same working conditions. If an error of
20° C. or more is noted, it is advisable to form a new junction, as the
discrepancy will probably become greater, being due to a change at the
hot junction. A small error, of the nature of 5 or 10° C., may be due
to “creep” in the indicator, which may be adjusted accordingly, or
a numerical correction may be made when taking a reading. An iron
protecting sheath may be saved from rapid oxidation by black-leading
once per week, which greatly prolongs its useful life, but should be
replaced immediately it becomes dangerously thin in any part. Coating
with aluminium powder also greatly prolongs the life of an iron sheath.
When used in lead baths, the immersed part, if of iron or steel, should
be bored from the solid, and left thick at the portion opposite the
surface of the lead, where most corrosion occurs. A graphite tube,
or one made of a composition containing graphite, is often useful in
cases where iron is readily corroded, and can be used to much higher
temperatures.
When a number of instruments are in use, it is advisable to keep a
standard pyrometer for checking purposes, preferably one which has been
certified by the National Physical Laboratory. In conducting a test,
the couples, with protecting-tubes removed, may be placed in the tube
of an electric furnace of the type shown in fig. 29, in close proximity
with the standard junction. On raising the temperature gradually, the
readings of each working instrument may be compared with the standard,
and the necessary corrections discovered. Care must be taken to prevent
contact with the furnace tube, and this may be accomplished by passing
the wires through an asbestos stopper fitted into the end of the tube.
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