Pyrometry: A Practical Treatise on the Measurement of High TemperaturesDarling, Charles R. (Charles Robert)
Science
Pyrometry: A Practical Treatise on the Measurement of High Temperatures
Darling, Charles R. (Charles Robert)
Pyrometry
When recorders are used the attendant should make himself thoroughly
conversant with the details of the mechanism, so as to be able to
remedy any minor ailments, which are, as a rule, easily cured. On no
account should an unskilled workman be trusted with recorders; it is
better and safer to keep these in the office, where they will not be
likely to be damaged or tampered with. All records should be kept
for future reference, properly dated, and labelled according to the
operations represented.
=Laboratory Uses of Thermo-electric Pyrometers.=—Numerous
operations carried out in muffle furnaces at prescribed temperatures
require no special precautions beyond those previously given.
In determining the melting points of metals or alloys, however,
a porcelain or silica sheath is inadvisable, as they are easily
corroded. An iron sheath is proof against some metals, but not
against others, and it is always safer to fix a thin fireclay sleeve,
closed at the end, over the part immersed. A sheath of graphite or
graphite composition may be used for temperatures above 1100° C.; and
occasionally a sheath bored from a thick arc-lamp carbon, coupled to
an iron tube beyond the heated part, will be found useful at high
temperatures. Alundum is useful up to 1600° C, and for temperatures of
this order the higher refractories such as silfrax and zirkite may also
be used to advantage.
[Illustration: FIG. 28.—DIFFERENTIAL METHOD FOR DETERMINING CRITICAL
POINTS OF STEEL.]
The determination of the “critical” points of steel call for special
mention. In cooling down a mass of steel the fall of temperature is
arrested at one or more points, observations of which are frequently
of service in deciding the subsequent treatment of the steel. A
method commonly employed is known as the “differential method,” and
is indicated in fig. 28. The sample of steel, A, is placed side by
side with a piece of nickel, B, of equal dimensions, in the tube of
an electric furnace. A naked junction, C, is placed in a hole drilled
in A, and is connected to the galvanometer G, which is calibrated to
read temperatures. A two-junction circuit, formed of a junction D
placed in the hole in A, and another junction E located in the hole in
B, are connected to a delicate galvanometer H. The furnace is heated
until the galvanometer G indicates 900° C., when the arrangement is
allowed to cool. As A and B, under normal circumstances, cool at an
equal rate, the junctions D and E will be at the same temperature, and
no deflection will be observed on H. When, owing to recalescence, the
cooling of A is arrested, B, not being thus affected, will continue to
cool, thus producing a difference between the temperatures of D and E,
and consequently a deflection on H. The temperature of A at the time
this occurs is read off on G.
[Illustration: FIG. 29.—ELECTRIC TUBE-FURNACE.]
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